Pesticide Analytical Manual Vol I page 102 D: Handling Samples for Special Analyses 1/94 102 E: Retention of Reserve portions 1/94 References 102-6 1/94 103: Method Application in Regulatory Analysi 109 A: Introduction 1031 1/94 103 B: Choice of Method 103-11/94 PAM 103-1 1/94 Other“ Official” Method 10321/94 Other Published method 1032 1/94 103 C: Tentative Identification 103-31/94 103 D: Residue Quantitation 103-3 1/94 103 E: Confirmation of Identity 103-41/94 103 F: Documentation 1036 Analytical Reports 103- 1/94 Chromatograms 103-7 1/94 Chromatographic Data 103-71/94 103-8 1/94 104 Analytical Results 104 A: Introduction 104-1 104 B: Reporting 104-1 1/94 Portion of Commodity 104-1 Nature of the residue 10421/9 Residues measured from derivative 1/94 or Breakdown Product Significant figures 10431/94 104-3 1/94 Confirmation 104-41/94 104 C: Determining Compliance with Regulations 104-4 1/94 General Rule for Multicomponent Residues 104-4 1/94 Special Situations 104-41/94 References 104-5 1/94 105 Analytical Limits of Quantitation 105 A: Definition 105-110/97 105 B: Calculation 105-110/97 105 C: Implementation 105210/97 105 D: Factors Affecting Target Limits of Quantitation 105-2 10/97 1002 Transmit N4: 905a16/9?1SECTION 100 Transmittal No. 98-1 (10/97) 100–2 Form FDA 2905a (6/92) Pesticide Analytical Manual Vol. I page date 102 D: Handling Samples for Special Analyses 102-6 1/94 102 E: Retention of Reserve Portions 102-6 1/94 References 102-6 1/94 103: Method Application in Regulatory Analysis 103 A: Introduction 103-1 1/94 103 B: Choice of Method 103-1 1/94 PAM 103-1 1/94 Other “Official” Methods 103-2 1/94 Other Published Methods 103-2 1/94 103 C: Tentative Identification 103-3 1/94 103 D: Residue Quantitation 103-3 1/94 103 E: Confirmation of Identity 103-4 1/94 103 F: Documentation 103-6 1/94 Analytical Reports 103-6 1/94 Chromatograms 103-7 1/94 Chromatographic Data 103-7 1/94 References 103-8 1/94 104: Analytical Results 104 A: Introduction 104-1 1/94 104 B: Reporting 104-1 1/94 Portion of Commodity 104-1 1/94 Nature of the Residue 104-2 1/94 Residues Measured from Derivative 104-2 1/94 or Breakdown Product Significant Figures 104-3 1/94 Trace 104-3 1/94 Confirmation 104-4 1/94 104 C: Determining Compliance with Regulations 104-4 1/94 General Rule for Multicomponent Residues 104-4 1/94 Special Situations 104-4 1/94 References 104-5 1/94 105: Analytical Limits of Quantitation 105 A: Definition 105-1 10/97 105 B: Calculation 105-1 10/97 105 C: Implementation 105-2 10/97 105 D: Factors Affecting Target Limits of Quantitation 105-2 10/97