l156 Journal of the American Ceramic Society--Sauder and Lamon Vol. 90. No. 4 Advanced Technical Ceramics--Ceramic Composites, Methods of Tests fo Microstructure Stability and Monoxide and argon ong.G. Hollon, C. Labrugere, M. Lahaye, A. Guette, J. L. BruneeL JH. M. Yun and J.A. Dic c简 he Tensile, Creep, and Rup- of Nearly Stoichiomet ture Strength Properties of Sto ;NASA/M-1999-209284 371-81020 I7M. H. Berger, N. Hochet, and A. R. Bunsell "Microstructure and Thermo- A. DiCarlo and H. M. Yun "Microstructural Factors Affecting Creep mechanical Stability of a Low-Oxygen Nicalon Fibre, "J. Microsc. Rupture Failure of Ceramic Fibers and Co (ISN.Hochet, M. H. Berger, and A.R.Bunsell, "Microstructural Evolution of A. Piant, A. Bunsell, and D. Ormston. pp 81-4, ""Comporten the Latest Generation eter SiC-Based Fibres Tested at High Tem haute temperature des fibres Sic de derniere generation, Groupe Francais de la Ceramique(French ceramic group). Annual Meeting. March 16-18. 2004. Bor- Ishikawa, T. Sato, Y. Tanaka, and M. Suzuki," A Thermally Conductive Sca- olx rais Pbo and Its Fiber-Bounded Ceramic, Ceram. Eng. Sci G. Langdon, ""Grain Boun Deformation Process 101-25in Applied Science Publishers, Barking, 1981 IC Sauder. J. Lamon. and R. Pailler"The Tensile Behavior of Carbon fibers iny. o rs me and w. , kingery, "Grain Boundary Segregation in Alumin. High Temperatures Up to 2400-C,Carbon, 42, 715-25(2004) 2T. L. Francis and R. L. Coble. "Creep of Polycrystalline Silicon Carbide. J. L. Chermant and F. Osterstock. ""Creep Behaviour of Sic-Al Materials. Mater.Sci.Eng.71,147-57(1985) hari and M.R. Notis."Interpretation of High-Temperature K. Schnurer. G. Grathwohl and F. Thummler "Kriechverhalten Verschied- Creep of SiC by Deformation Mapping Techniques. "Mater. Sci. Eng, 27. 83-8 P. Rocabois,"Stabilite thermochimique des composites ceramique base Sic =G Morscher, H. M. Yun, and J. C Goldsby, "Bend Stress Relaxation and approche thermodynamique et experimentale du systeme Si-O-C-N These de of Ceramics. Edited by R. C. Bradt, C. A. Brookes, and J. L 4P Grieveson and C. B. Alcock, The Thermodynamics of Metal Silicides and Sil ohl, Th. Reets, and F. Thummler, Creep of Hot-Pressed and Sin- onov, Plemum Press Handbooks of Higl-Temperature Materials: tered Sic With Different Sintering Additives, Sci. Ceram. 11. 425-31(1981) perties Index, N. 2. Plenum Press. New York. 1964. 3J. D. Hong. M. H Hon, and R F. Davis, "Sell-Diffusion in Alpha and Beta D. L. Hildenbrand and w. F. Hall"The D ilicon Carbide, Cerarmrgia Int, 514] 155-60(1979) Carbide and the Heat of Sublimation of Boron, J. Phys. Che, 6851989-93(1964) veno. J. Li Chaumont."Diffusion of C and 2 J E Sheehan, "Ceramic Coatings for Carbon Materials": Pp. 57-98, Pro- Implanted lons in iC, Mater Sci Eng. B111331-6(1992. ceedings of Fourth Annual Conference, "" Recent progress into carbon-carbon oble. ""Self-Diffusion in Silicon Carbide 4C. B. Alcock,"Zirconium: Physico-Chemical properties of its Compounds M. H. Hon and R. F. Davis, "Self-Diffusion of C in Polycrystalline B-Sic J. Mater.Sci.,14.241l-2l(1979 1 amics properties", pp. 7-63, Atomic I 6(IAEA-Vienne. 1976. 阝-siC,"J. Mater.Si,15,2073-80(198 4D. R. Lide, Handbook of Chemistry and Physics. 7Ist edition, CRC Press. 3R. Kossowsky, "Cyclic Fatigue of Hot-Pressed Si3N4."J.Am. Ceram.Soc S C. Singhal, "Thermodynamic Analysis of the High-Temperature Stability of murgia int.23123-130 P. L Farnsworth and R.L. Coble. "Deformation Behavior of dense poly- G. Hollon. ""Fibres ceramique a base crystalline SiC,J. Am. Ceram. Soc, 49[5] 264-8(Is d'oxygene. These de universite de Bordeaux 1, 1995.15Advanced Technical Ceramics—Ceramic Composites, Methods of Tests for Reinforcement—Part 6: Determination of Tensile Properties of Filament at High Temperature, European standard CENTC 184, ENV1007-6, 2001. 16S. M. Dong, G. Chollon, C. Labrugere, M. Lahaye, A. Guette, J. L. Bruneel, M. Couzi, R. Naslain, and D. L. Jiang, ‘‘Characterization of Nearly Stoichiomet￾ric SiC Ceramic Fibres,’’ J. Mater. Sci., 36, 2371–81 (2001). 17M. H. Berger, N. Hochet, and A. R. Bunsell, ‘‘Microstructure and Thermo￾Mechanical Stability of a Low-Oxygen Nicalon Fibre,’’ J. Microsc., 177 [3] 230–41 (1994). 18N. Hochet, M. H. Berger, and A. R. Bunsell, ‘‘Microstructural Evolution of the Latest Generation of Small-Diameter SiC-Based Fibres Tested at High Tem￾peratures,’’ J. Microsc., 185 [2] 243–58 (1997). 19T. Ishikawa, T. Sato, Y. Tanaka, and M. Suzuki, ‘‘A Thermally Conductive SiC-Polycrystalline Fiber and Its Fiber-Bounded Ceramic,’’ Ceram. Eng. Sci. Proc., 22 [3] 471–80 (2001). 20B. T. Kelly, Physics of Graphite. Applied Science Publishers, Barking, 1981. 21C. Sauder, J. Lamon, and R. Pailler, ‘‘The Tensile Behavior of Carbon Fibers at High Temperatures Up to 24001C,’’ Carbon, 42, 715–25 (2004). 22T. L. Francis and R. L. Coble, ‘‘Creep of Polycrystalline Silicon Carbide,’’ J. Am. Ceram. Soc., 51 [2] 115–6 (1968). 23V. Krishnamashari and M. R. Notis, ‘‘Interpretation of High-Temperature Creep of SiC by Deformation Mapping Techniques,’’ Mater. Sci. Eng., 27, 83–8 (1977). 24G. Morscher, H. M. Yun, and J. C. Goldsby, ‘‘Bend Stress Relaxation and Tensile Primary Creep of a Polycrystalline a-SiC Fiber’’; pp. 467–78 in Plastic Deformation of Ceramics, Edited by R. C. Bradt, C. A. Brookes, and J. L. Routbort, Plenum Press, New York, 1995. 25G. Grathwohl, Th. Reets, and F. Thummler, ‘‘Creep of Hot-Pressed and Sin￾tered SiC With Different Sintering Additives,’’ Sci. Ceram., 11, 425–31 (1981). 26J. D. Hong, M. H. Hon, and R. F. Davis, ‘‘Self-Diffusion in Alpha and Beta Silicon Carbide,’’ Ceramurgia Int., 5 [4] 155–60 (1979). 27P. Eveno, J. Li, A. M. Huntz, and J. Chaumont, ‘‘Diffusion of 13C and 29Si Implanted Ions in SiC,’’ Mater. Sci. Eng., B11 [1–4] 331–6 (1992). 28R. N. Ghoshtagore and R. L. Coble, ‘‘Self-Diffusion in Silicon Carbide,’’ Phys. Rev., 143 [2] 623–6 (1966). 29M. H. Hon and R. F. Davis, ‘‘Self-Diffusion of 14C in Polycrystalline b-SiC,’’ J. Mater. Sci., 14, 2411–21 (1979). 30M. H. Hon, Davis, and E. Newbury, ‘‘Self-Diffusion of 30Si in Polycrystalline b-SiC,’’ J. Mater. Sci., 15, 2073–80 (1980). 31R. Kossowsky, ‘‘Cyclic Fatigue of Hot-Pressed Si3N4,’’ J. Am. Ceram. Soc., 56, 531 (1973). 32P. L. Farnsworth and R. L. Coble, ‘‘Deformation Behavior of Dense Poly￾crystalline SiC,’’ J. Am. Ceram. Soc., 49 [5] 264–8 (1966). 33R. Bodet, J. Lamon, N. Jia, and R. E. Tressler, ‘‘Microstructure Stability and Creep Behavior of Si–C–O (Nicalon) Fibers in Carbon Monoxide and Argon En￾vironments,’’ J. Am. Ceram. Soc., 79 [10] 2673–83 (1996). 34H. M. Yun and J. A. DiCarlo, ‘‘Comparison of the Tensile, Creep, and Rup￾ture Strength Properties of Stoichiometric SiC Fibers’’; NASA/TM-1999-209284 report, July, 1999. 35J. A. DiCarlo and H. M. Yun, ‘‘Microstructural Factors Affecting Creep￾Rupture Failure of Ceramic Fibers and Composites,’’ Ceram. Mater. Syst. Com￾pos. Struct., 119–34 (1998). 36A. Piant, A. Bunsell, and D. Ormston. pp. 81–4, ‘‘Comportement me´canique a` haute temperature des fibres SiC de dernie`re generation,’’ Groupe Fran@ais de la Ce´ramique (French ceramic group), Annual Meeting, March 16–18, 2004, Bor￾deaux, 2004. 37T. G. Langdon, ‘‘Grain Boundary Deformation Process’’; pp. 101–25 in Deformation of Ceramic Materials, Edited by R. C. Bradt and R. E. Tressler, Plenum Press, New York, 1975. 38Y. O. Tajima and W. D. Kingery, ‘‘Grain Boundary Segregation in Alumin￾ium-Doped Silicon Carbide,’’ J. Mater. Sci., 17, 2289–97 (1982). 39J. L. Chermant and F. Osterstock, ‘‘Creep Behaviour of SiC–Al Materials,’’ Mater. Sci. Eng., 71, 147–57 (1985). 40K. Schnurer, G. Grathwohl, and F. Thummler, ‘‘Kriechverhalten Verschied￾ener SiC-Werkstoffe,’’ Sci. Ceram., 10, 645–50 (1980). 41P. Rocabois, ‘‘Stabilite´ thermochimique des composites ceramiques base SiC approche thermodynamique et expe´rimentale du syste`me Si–O–C–N’’; The`se de l’universite´ de Bordeaux I, 1993. 42P. Grieveson and C. B. Alcock, The Thermodynamics of Metal Silicides and Sil￾icon Carbide, Special Ceramic 1960, pp. 183. Academic Press Inc, New York, 1960. 43G. V. Samsonov, Plenum Press Handbooks of High-Temperature Materials: Properties Index, N. 2. Plenum Press, New York, 1964. 44D. L. Hildenbrand and W. F. Hall, ‘‘The Decomposition Pressure of Boron Carbide and the Heat of Sublimation of Boron,’’ J. Phys. Chem., 68 [5] 989–93 (1964). 45J. E. Sheehan, ‘‘Ceramic Coatings for Carbon Materials’’; pp. 57–98, Pro￾ceedings of Fourth Annual Conference, ‘‘Recent progress into carbon-carbon composites,’’ 1987. 46C. B. Alcock, ‘‘Zirconium: Physico-Chemical properties of its Compounds and Alloys—I. Thermodynamics properties’’; pp. 7–63, Atomic Energy Review— special issue no 6 (IAEA—Vienne), 1976. 47D. R. Lide, Handbook of Chemistry and Physics, 71st edition, CRC Press, Boca Raton, FL, 1990-1991. 48S. C. Singhal, ‘‘Thermodynamic Analysis of the High-Temperature Stability of Silicon Nitride and Silicon Carbide,’’ Ceramurgia Int., 2 [3] 123–130 (1970). 49G. Chollon, ‘‘Fibres ce´ramiques a` base de carbure de silicium et a` faible taux d’oxyge`ne, The`se de l’universite´ de Bordeaux I, 1995. & 1156 Journal of the American Ceramic Society—Sauder and Lamon Vol. 90, No. 4