l150 Journal of the American Ceramic Society--Sauder and Lamon Vol. 90. No. 4 sA3(1) (2) Fig. 5. Scanning electron microscope micrographs of the cross sections of (a) Hi-Nicalon. (b)Hi-Nicalon S(c) Tyranno SA3(1), and(d) Tyranno SA3 produces substantial basal plane shear. Furthermore, the mag- It is worth mentioning that primary creep was more signifi nitude of the viscoelastic response of carbon fibers under tension cant in those fibers that contained a large amount of carbon(Hi- depends on the orientation of the graphitic planes. It increases Nicalon). This supports the above carbon deformation-driven with the fraction of graphitic planes with a large angle to loading mechanism direction(isotropic carbon). By contrast, it is limited in the ani Although the Hi-Nicalon and SA3 (1) fibers possessed the sotropic fibers, in which most of the graphitic planes are orient same fraction of carbon, Hi-Nicalon fiber showed a larger sen- ed parallel to the loading direction. In SiC fibers, the orientation sitivity to creep. This discrepancy can be attributed to grain size of graphitic planes is influenced by grain-boundary distribution. which is much smaller in the Hi- Nicalon fiber. It could also Thus, graphitic planes can take on all orientations. Further- be related to the structure of carbon, which displayed a better more, it was indicated earlier that the carbon present in these rganization in the SA3(1) fiber (smaller distance between iC fibers consists of stacks of a few graphitic planes. As a con- two successive layers: doo), as a result of a higher-processing sequence, primary creep may involve deformation of carbon at temperature. A low doog implies a larger stiffness and smaller grain boundaries and grain sliding due to basal plane shear deformationsproduces substantial basal plane shear.20 Furthermore, the magnitude of the viscoelastic response of carbon fibers under tension depends on the orientation of the graphitic planes.21 It increases with the fraction of graphitic planes with a large angle to loading direction (isotropic carbon). By contrast, it is limited in the anisotropic fibers, in which most of the graphitic planes are oriented parallel to the loading direction. In SiC fibers, the orientation of graphitic planes is influenced by grain-boundary distribution. Thus, graphitic planes can take on all orientations. Furthermore, it was indicated earlier that the carbon present in these SiC fibers consists of stacks of a few graphitic planes. As a consequence, primary creep may involve deformation of carbon at grain boundaries and grain sliding due to basal plane shear. It is worth mentioning that primary creep was more signifi- cant in those fibers that contained a large amount of carbon (HiNicalon). This supports the above carbon deformation-driven mechanism. Although the Hi-Nicalon and SA3 (1) fibers possessed the same fraction of carbon, Hi-Nicalon fiber showed a larger sensitivity to creep. This discrepancy can be attributed to grain size, which is much smaller in the Hi-Nicalon fiber. It could also be related to the structure of carbon, which displayed a better organization in the SA3 (1) fiber (smaller distance between two successive layers: d002), as a result of a higher-processing temperature. A low d002 implies a larger stiffness and smaller deformations. (a) Hi-Nicalon (b) Hi-Nicalon S SA3 (1) SA3 (2) (c) (d) Zoom Fig. 5. Scanning electron microscope micrographs of the cross sections of (a) Hi-Nicalon, (b) Hi-Nicalon S, (c) Tyranno SA3 (1), and (d) Tyranno SA3 (2) fibers. 1150 Journal of the American Ceramic Society—Sauder and Lamon Vol. 90, No. 4