正在加载图片...
November 200 Carbothermal Synthesis of BN Coatings on SiC 1837 -P B Mirkarimi, K. F. McCarty, and D. L. Medlin, "Review of Advances in Cubic 2D. Golberg, Y. Bando, L. Bourgeois, R. Ma, K. Ogawa, K. Kurashima, and T. Boron Nitride Film Synthesis, Mater. Sci. Eng, R21, 47-100(1997) tube, Nanocable and Nanocone, Mater. Res. Soc. Symp otzbucher, w, Pfleging, M. Me A. Wesner, and E. w. Kreutz, Proc,706,Z23.1-Z2.3.10(2002) Structure and Chemical Composition of BN Thin Films Grown by Pulsed-Laser S. Ulrich, T BlackglasM Ceramic Matrix Composite Properties, "Ceram. Eng. Sci. Proc., 15, M. B. Mekki, M, A Djouadi, E. Guiot, V. Mortet, J. Pascallon, V. Stambouli, D Bouchier, N. Mestres, and G Nouet, "Structure Investigation of BN Films Grown by L. S. Brown and R. E. Partch,"" Boron Nitride Coatings on Silicon Carbide Means of Polarised IR and Raman Spectroscopy, 2M. Avella, E. Martuscelli, M. Raimo, R. E. Partch, S. G. Gangolli, and B Coat. Technol,116-1993-99(1999 Pascucci,"Polypropylene Reinforced with Silicone Carbide W R. D. Veltri and F. S. Galasso, "Chemical-Vapor-Ir itride,and Silicon Carbide Matrix Composites,J.An 二) Behlau, D. Koch, G. Grathwohl, S. Welz, M. J. McNallan, L. Chen, and Y Gogotsi,""Mechanical Properties of Carbon Coated Ceramic Fibers, 27th Ann ocoa Beach Conference on Advanced Ceramics and Composites, Ceram. Eng. Sci. R N. Singh and M. K. Brun, "Effect of Boron Nitride Coating on Fiber-Matrix Interactions, Ceram. Eng. Sci. Proc., 8[7-8]636-43(1987). Y.G. Gogotsi, "Formation of Carbon Coatings on Carbide Fibers and particles Filipuzzi, G. Camus, R. Naslain, and T. Imamura,"( by Dispropor ns. NATO AS/ Ser.43.217- m.Soc,77[2]459-66(1994) patinas or IJ. D. Cawley, "Effect of Interphase Carbon Thickness on Environmental in Halogens and Supercritical Water,Ceram. Eng. Sci. Proc., 19, 87-94(1998) 377-84 in Ceramic Transactions, Vol 58, High-Temperature Ceramic-Matrir Com- IC F. Windisch Jr, C. H. Henager Jr, G. D. Springer, and R H. Jones, "Oxidation The Minerals, Metals an of the Carbon Interface in Nicalon-Fiber-Reinforced Silicon Carbide Composite, 33Y. Gogotsi, I. D Jeon, and M. J. McNallan, "Carbon Coatings Produced by High J. Am. Ceram. Soc., 80 [3] 569-74(19 Temperature Chlorination of Silicon Carbide Ceramics, J. Mater. Chen,7 T. E. Steyer, F. W. Zok, and D. P. Walls, "Stress Rupture of an Enhanced Nicalon/Silicon Carbide Composite at Intermediate Temperature, "J. An. Ceram D. A Ersoy, M. MeNallan, Y Gogotsi, and A. Erdemir, "Tribological Properties Soc,8I8]2140-46(19989 of Carbon Coatings Produced by High Temperature Chlorination of Silicon Carbide, IG. N. Morscher, "Tensile Stress Rupture of SiC/Sicm Minicomposite Tribol.Tas.,43,809-15(2000) Carbon and Bo phase at Elevated Temperatures in Air,J.Am. 3R. Ma. Y. Bando, T. Sato, and K.Kurashima, th Morphology, and IY. G. Gogotsi, and M. Yoshimura, "Low-Temperature Oxidation, Hydrothermal 36Y. Bando, D. Golberg, M. Mitome, K. Kurashima, and T. Sato, " C to BN Corrosion, and Their Effects on properties of SiC(Tyranno)Fibers," J. Am. Ceram. Electron Microscopy, "Chem. Plys. Let, 346, 29-34(2001). J. E. Lane and A. R. Pebler"Failure Characteristics of Low dielectric Constant Z F. Zhou, I. Bello, V Kremnica, M. K. Fung, K. H. Lai, K. Y Li, C S. Le Ceramic Composites Reinforced with BN-Coated Fibers, "Ceram. Eng. Sci. Proc., 10 and S. T. Lee, "Formation of Cubie Boron Nitride Films on Nickel Substrates, Th id films,368,292-96(2000 I6J. Llorca and R. N. Singh, "Influence of Fiber and Interfacial Properties H Sachdev, R. Haubner, H. Noth, and B Lux, "Investigation of the c-BN/h-BN Fracture Behavior of Fiber-Reinforced Ceramic Composites, " J. Am. Ceram Soc., 74 Phase Transformation at Normal Pressure, Diamond Relat. Mater. 6, 286-92 12882-90(1991 (1997) R. Naslain, O. Dugne, A. Guette, J. Sevely, C. R. Brosse, J. P. Rocher, and J R Ma, Y. Bando, and T. Sato, "Coaxial Nanocables: Fe Nanowires Encapsu Cotteret, "Boron Nitride Interphase in Ceramic-Matrix Composites, J. Am. Ce in BN Nanotubes with Intermediate C Layers, "Chem. Phys. Lett., 350, 1-5(2001) Soc,74[102482-88(1991) 4H Nozaki and S Itoh, "Structural Stability of BC2N, ".. Phys. Chem. Solids, 5 e141-4 Shen, B J. Tan, w.S. Willis, F. S. Galasso, and S L, Suib, "Characterizatio ZMI Fiber/Silicon-Titanium-Carbon-Oxygen Matrix Composites, J. Am. Ceram. of Dip-Coated Boron Nitride on Silicon Carbide Fibers,.Am. Ceram Soc., 77 4 Soc,85[2]393-400(2002) 011-16(1994 Y G. Andreev, T. Lundstrom, R. K Harris, S. w. Oh, D. C. Apperley, and D.P. 42L. Shen, W.S. willis, F. S. Galasso, and S. L. Suib, "Coating of Boron Nitride interfaces on Ceramic Y arms from Boric Acid and Ammonia, "J Am Ceram Soc., 14 L. Andujar,"Micromechanical 43Y. Gogotsi, S. Welz, D. A. Ersoy, and M. J. McNallan, "Conversion of Silicon Properties of BN and B-CN Coatings Obtained by RF Plasma-Assisted CVD, Ca ystalline Diamond-Structured Carbon at Ambient Pressure, "Natwre Diamond Relat. Mater, 8, 423-27(1999). London,411,2838702001) opL. Phys. Lett., 74[20]2948- Ceramic Transactions, Vol. 148, Ceramic Nanomaterials and Nanotechnology I1. 2T. H. Tsai, T S. Yang, C L Cheng, and M. S. Wo of Boron Nit C)Films by Pulsed-DC Magnetron Sputtering, Chem Y Matsui, Y Sekikawa, T. Sato, T. Ishii, S. Isakawa, and K. Shii, "Formations Plys.,72,264-68(2001) of Rhombohedral Boron Nitride, as Revealed by TEM-Electron Energy Loss Cho and J. A. Charles,"Synthesis of Nitrogen Ceramic Powders by on and Nitridation, Part 3: Aluminum Nitride, " Mater. Sci. P. B. Mirkarimi, K. F. McCarty, and D. L. Medlin, "Review of Advances Cubic Boron Nitride Film Synthesis, "Mater. Sci. Eng, R21, 47-100(199 Un, "Carbothermal Reduction and Nitridation of Titanium 473. S. Ha and K. K Chawla, "Effect of SiC/BN Double Coating on Fiber Pullout in and Products, " J. Chem. Eng. Jpn., 31 [5]804-807(1998). Mullite Fibre/Mullite Matrix Composites, "J. Mater. Sci. Leff, 12, 84-86(1993) D2 P. B. Mirkarimi, K. F. McCarty, and D. L. Medlin, “Review of Advances in Cubic Boron Nitride Film Synthesis,” Mater. Sci. Eng., R21, 47–100 (1997). 3 T. Klotzbu¨cher, W. Pfleging, M. Mertin, D. A. Wesner, and E. W. Kreutz, “Structure and Chemical Composition of BN Thin Films Grown by Pulsed-Laser Deposition (PLD),” Appl. Surf. Sci., 86, 165–69 (1995). 4 S. Ulrich, T. Theel, J. Schwan, and H. Ehrhardt, “Magnetron-Sputtered Superhard Materials,” Surf. Coat. Technol., 97, 45–59 (1997). 5 M. B. Mekki, M. A. Djouadi, E. Guiot, V. Mortet, J. Pascallon, V. Stambouli, D. Bouchier, N. Mestres, and G. Nouet, “Structure Investigation of BN Films Grown by Ion-Beam-Assisted Deposition by Means of Polarised IR and Raman Spectroscopy,” Surf. Coat. Technol., 116–119, 93–99 (1999). 6 B. T. Kelly, Physics of Graphite. Applied Science, London, U.K., 1981. 7 R. D. Veltri and F. S. Galasso, “Chemical-Vapor-Infiltrated Silicon Nitride, Boron Nitride, and Silicon Carbide Matrix Composites,” J. Am. Ceram. Soc., 73 [7] 2137–40 (1990). 8 R. N. Singh and M. K. Brun, “Effect of Boron Nitride Coating on Fiber–Matrix Interactions,” Ceram. Eng. Sci. Proc., 8 [7–8] 636–43 (1987). 9 L. Filipuzzi, G. Camus, R. Naslain, and T. Ymamura, “Oxidation Mechanisms and Kinetics of 1D SiC/SiC Composite Materials: I, An Experimental Approach,” J. Am. Ceram. Soc., 77 [2] 459–66 (1994). 10J. D. Cawley, “Effect of Interphase Carbon Thickness on Environmental Resistance of Continuous Fiber-Reinforced Ceramic Matrix Composites”; pp. 377–84 in Ceramic Transactions, Vol. 58, High-Temperature Ceramic-Matrix Composites II. American Ceramic Society, Westerville, OH, 1995. 11C. F. Windisch Jr., C. H. Henager Jr., G. D. Springer, and R. H. Jones, “Oxidation of the Carbon Interface in Nicalon-Fiber-Reinforced Silicon Carbide Composite,” J. Am. Ceram. Soc., 80 [3] 569–74 (1997). 12T. E. Steyer, F. W. Zok, and D. P. Walls, “Stress Rupture of an Enhanced Nicalon/Silicon Carbide Composite at Intermediate Temperature,” J. Am. Ceram. Soc., 81 [8] 2140–46 (1998). 13G. N. Morscher, “Tensile Stress Rupture of SiCf/SiCm Minicomposites with Carbon and Boron Nitride Interphase at Elevated Temperatures in Air,” J. Am. Ceram. Soc., 80 [8] 2029–42 (1997). 14Y. G. Gogotsi, and M. Yoshimura, “Low-Temperature Oxidation, Hydrothermal Corrosion, and Their Effects on properties of SiC (Tyranno) Fibers,” J. Am. Ceram. Soc., 78 [6] 1439–50 (1995). 15J. E. Lane and A. R. Pebler, “Failure Characteristics of Low Dielectric Constant Ceramic Composites Reinforced with BN-Coated Fibers,” Ceram. Eng. Sci. Proc., 10 [9–10] 1213–22 (1989). 16J. Llorca and R. N. Singh, “Influence of Fiber and Interfacial Properties on Fracture Behavior of Fiber-Reinforced Ceramic Composites,” J. Am. Ceram. Soc., 74 [11] 2882–90 (1991). 17R. Naslain, O. Dugne, A. Guette, J. Sevely, C. R. Brosse, J. P. Rocher, and J. Cotteret, “Boron Nitride Interphase in Ceramic-Matrix Composites,” J. Am. Ceram. Soc., 74 [10] 2482–88 (1991). 18T. Ogasawara, T. Ishikawa, Y. Ohsawa, Y. Ochi, and S. Zhu, “Tensile Creep Behavior and Thermal Stability of Orthogonal Three-Dimensional Woven TyrannoTM ZMI Fiber/Silicon–Titanium–Carbon–Oxygen Matrix Composites,” J. Am. Ceram. Soc., 85 [2] 393–400 (2002). 19Y. G. Andreev, T. Lundstrom, R. K. Harris, S. W. Oh, D. C. Apperley, and D. P. Thompson, “On the Nature of Boron–Carbon–Nitrogen Compounds Synthesized from Organic Precursors,” J. Alloys Compd., 227, 102–108 (1995). 20M. C. Polo, E. Martinez, J. Esteve, and J. L. Andujar, “Micromechanical Properties of BN and B–CN Coatings Obtained by RF Plasma-Assisted CVD,” Diamond Relat. Mater., 8, 423–27 (1999). 21J. Yu and E. G. Wang “Turbostratic Boron Carbonitride Film and Its FieldEmitting Behavior,” Appl. Phys. Lett., 74 [20] 2948–50 (1999). 22T. H. Tsai, T. S. Yang, C. L. Cheng, and M. S. Wong, “Synthesis and Properties of Boron Nitride (BN:C) Films by Pulsed-DC Magnetron Sputtering,” Mater. Chem. Phys., 72, 264–68 (2001). 23Y. W. Cho and J. A. Charles, “Synthesis of Nitrogen Ceramic Powders by Carbothermal Reduction and Nitridation, Part 3: Aluminum Nitride,” Mater. Sci. Technol., 7 [6] 495–504 (1991). 24C. K. Yu and C. I. Un, “Carbothermal Reduction and Nitridation of Titanium Dioxide—Intermediates and Products,” J. Chem. Eng. Jpn., 31 [5] 804–807 (1998). 25D. Golberg, Y. Bando, L. Bourgeois, R. Ma, K. Ogawa, K. Kurashima, and T. Sato, “Boron Nitride Nanotube, Nanocable and Nanocone,” Mater. Res. Soc. Symp. Proc., 706, Z2.3.1-Z2.3.10 (2002). 26S. S. Campbell and S. T. Gonczy, “In Situ Formation of Boron Nitride Interfaces on NextelTM 312 Continuous Ceramic Fiber: I, Nitriding Process and BlackglasTM Ceramic Matrix Composite Properties,” Ceram. Eng. Sci. Proc., 15, 327–36 (1994). 27I. S. Brown and R. E. Partch, “Boron Nitride Coatings on Silicon Carbide Whiskers,” Mater. Res. Soc. Symp. Proc., 458, 421 (1996). 28M. Avella, E. Martuscelli, M. Raimo, R. E. Partch, S. G. Gangolli, and B. Pascucci, “Polypropylene Reinforced with Silicone Carbide Whiskers,” J. Mater. Sci., 32 [9] 2411–16 (1997). 29G. Behlau, D. Koch, G. Grathwohl, S. Welz, M. J. McNallan, L. Chen, and Y. Gogotsi, “Mechanical Properties of Carbon Coated Ceramic Fibers,” 27th Annual Cocoa Beach Conference on Advanced Ceramics and Composites, Ceram. Eng. Sci. Proc., in press. 30Y. G. Gogotsi, “Formation of Carbon Coatings on Carbide Fibers and Particles by Disproportionation Reactions,” NATO ASI Ser., 43, 217–30 (1997). 31Y. G. Gogotsi, S. Welz, J. Daghfal, M. J. McNallan, I. D. Jeon, K. G. Nickel, and T. Kraft, “Formation of Carbon Coatings on SiC fibers by Selective Etching in Halogens and Supercritical Water,” Ceram. Eng. Sci. Proc., 19, 87–94 (1998). 32M. McNallan, Y. Gogotsi, and D. Erosy, “Reaction Formed Coatings for SiC Fibers in Ceramic Matrix Composites”; pp. 351–59 in Elevated Temperature Coatings: Science and Technology III. Edited by J. M. Hampikian and N. B. Dahorte. The Minerals, Metals and Materials Society (TMS), Warrendale, PA, 1999. 33Y. Gogotsi, I. D. Jeon, and M. J. McNallan, “Carbon Coatings Produced by High Temperature Chlorination of Silicon Carbide Ceramics,” J. Mater. Chem., 7 [9] 1841–48 (1997). 34D. A. Ersoy, M. McNallan, Y. Gogotsi, and A. Erdemir, “Tribological Properties of Carbon Coatings Produced by High Temperature Chlorination of Silicon Carbide,” Tribol. Trans., 43, 809–15 (2000). 35R. Ma, Y. Bando, T. Sato, and K. Kurashima, “Growth Morphology, and Structure of Boron Nitride Nanotubes,” Chem. Mater., 13, 2965–71 (2001). 36Y. Bando, D. Golberg, M. Mitome, K. Kurashima, and T. Sato, “C to BN Conversion in Multi-walled Nanotubes as Revealed by Energy-filtering Transmission Electron Microscopy,” Chem. Phys. Lett., 346, 29–34 (2001). 37Z. F. Zhou, I. Bello, V. Kremnican, M. K. Fung, K. H. Lai, K. Y. Li, C. S. Lee, and S. T. Lee, “Formation of Cubic Boron Nitride Films on Nickel Substrates,” Thin Solid Films, 368, 292–96 (2000). 38H. Sachdev, R. Haubner, H. No¨th, and B. Lux, “Investigation of the c-BN/h-BN Phase Transformation at Normal Pressure,” Diamond Relat. Mater., 6, 286–92 (1997). 39R. Ma, Y. Bando, and T. Sato, “Coaxial Nanocables: Fe Nanowires Encapsulated in BN Nanotubes with Intermediate C Layers,” Chem. Phys. Lett., 350, 1–5 (2001). 40H. Nozaki and S. Itoh, “Structural Stability of BC2N,” J. Phys. Chem. Solids, 57 [1] 41–49 (1996). 41L. Shen, B. J. Tan, W. S. Willis, F. S. Galasso, and S. L. Suib, “Characterization of Dip-Coated Boron Nitride on Silicon Carbide Fibers,” J. Am. Ceram. Soc., 77 [4] 1011–16 (1994). 42L. Shen, W. S. Willis, F. S. Galasso, and S. L. Suib, “Coating of Boron Nitride interfaces on Ceramic Yarns from Boric Acid and Ammonia,” J. Am. Ceram. Soc., 14 [7–8] 556–62 (1993). 43Y. Gogotsi, S. Welz, D. A. Ersoy, and M. J. McNallan, “Conversion of Silicon Carbide to Crystalline Diamond-Structured Carbon at Ambient Pressure,” Nature (London), 411, 283–87 (2001). 44L. Chen, H. Ye, and Y. Gogotsi, “Nanocrystalline BN/C Coating on SiC,” in Ceramic Transactions, Vol. 148, Ceramic Nanomaterials and Nanotechnology II. American Ceramic Society, Westerville, OH, in press. 45Y. Matsui, Y. Sekikawa, T. Sato, T. Ishii, S. Isakawa, and K. Shii, “Formations of Rhombohedral Boron Nitride, as Revealed by TEM—Electron Energy Loss Spectroscopy,” J. Mater. Sci., 16, 1114–16 (1981). 46P. B. Mirkarimi, K. F. McCarty, and D. L. Medlin, “Review of Advances in Cubic Boron Nitride Film Synthesis,” Mater. Sci. Eng., R21, 47–100 (1997). 47J. S. Ha and K. K. Chawla, “Effect of SiC/BN Double Coating on Fiber Pullout in Mullite Fibre/Mullite Matrix Composites,” J. Mater. Sci. Lett., 12, 84–86 (1993). November 2003 Carbothermal Synthesis of BN Coatings on SiC 1837