Pesticide Analytical Manual Vol. I date 40411/94 Reference standards 4041 /94 Steps of the method 40411/94 Validation 4043 1/94 Extraction with methanol transfer to 40451/94 Extraction with methanol, removal of oil with 404-7 1/94 hexane, transfer to methylene chloride Extraction with methanol, removal of oil with 404-8 1/94 thylene chloride DL5 HPLC, Ion Pair Mobile Phase, UV and 4049 1/94 Fluorescence detector DL6 HPLC, Concentrated Ion Pair Mobile Phase, 404-12 1/9 UV and Fluorescence Detector DL7 HPLC, Ion Pair Mobile Phase, Changes in 404141/94 Confirmation 404141/94 res 101-a Method for N-Methylcarbamates 401-2 1/94 401-b Vacuum Rotary Evaporator 401-31/94 HPLC System for Determination of 401-91/94 N-Methylcarbamates 401-d HPLC Chromatogram of carbamates 401-121/94 and metabolites 402-a Method for Acids and Phenols 1/94 402-b Delivery Tube apparatus 402-3 1/9 403-a Method for Phenylureas 403-2 1/94 403b HPLC System for Determination of 403-71/94 Phenylurea Herbicides 403-c HPLC Chromatograms of carrot extract 403-101/94 403-d Chromatographic Pattern Comparison 403-111/94 404a lethod for benzimidazoles 0421/94 404-b Chromatograms of Benzimidazole Compounds 4104-12 9/96 404-C Effect of Ion Pairing Solution Concentration 404-18 1/94 on Chromatography of MBC Tables 401-a: Recovery of Chemicals Through Method 401 401-a-1 9/96 401-b: Recovery of Chemicals Through Method 401 401-b-l 9/96 402-a: Recovery of Chemicals Through Method 402 402-a-l 9/96 (El-E7 +Cl+DGl or DG% or DG4) 403a: Recovery of Chemicals Through Method 403 403-a-1 9/96 (El +Cl+ dl3 and DL4) Form FDA 2905a (6/92 400-3Pesticide Analytical Manual Vol. I 400–3 Transmittal No. 96-E1 (9/96) Form FDA 2905a (6/92) page date Applicability 404-1 1/94 Reference Standards 404-1 1/94 Steps of the Method 404-1 1/94 Validation 404-3 1/94 E1 Extraction with methanol, transfer to 404-5 1/94 methylene chloride E2 Extraction with methanol, removal of oil with 404-7 1/94 hexane, transfer to methylene chloride E3 Extraction with methanol, removal of oil with 404-8 1/94 methylene chloride, transfer to methylene chloride DL5 HPLC, Ion Pair Mobile Phase, UV and 404-9 1/94 Fluorescence Detector DL6 HPLC, Concentrated Ion Pair Mobile Phase, 404-12 1/94 UV and Fluorescence Detector DL7 HPLC, Ion Pair Mobile Phase, Changes in 404-14 1/94 Detector Settings Confirmation 404-14 1/94 Figures 401-a Method for N-Methylcarbamates 401-2 1/94 401-b Vacuum Rotary Evaporator 401-3 1/94 401-c HPLC System for Determination of 401-9 1/94 N-Methylcarbamates 401-d HPLC Chromatogram of Carbamates 401-12 1/94 and Metabolites 402-a Method for Acids and Phenols 402-2 1/94 402-b Delivery Tube Apparatus 402-3 1/94 403-a Method for Phenylureas 403-2 1/94 403-b HPLC System for Determination of 403-7 1/94 Phenylurea Herbicides 403-c HPLC Chromatograms of Carrot Extract 403-10 1/94 403-d Chromatographic Pattern Comparison 403-11 1/94 404-a Method for Benzimidazoles 404-2 1/94 404-b Chromatograms of Benzimidazole Compounds 404-12 9/96 404-c Effect of Ion Pairing Solution Concentration 404-13 1/94 on Chromatography of MBC Tables 401-a: Recovery of Chemicals Through Method 401 401-a–1 9/96 (E1-E2 + C1 + DL1) 401-b: Recovery of Chemicals Through Method 401 401-b–1 9/96 (E1-E2 + C1 + DL2) 402-a: Recovery of Chemicals Through Method 402 402-a–1 9/96 (E1-E7 + C1 + DG1 or DG3 or DG4) 403-a: Recovery of Chemicals Through Method 403 403-a–1 9/96 (E1 + C1 + DL3 and DL4)