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KAYA et al.: FABRICATION AND CHARACTERISATION OF ALUMINA CERAMIC MATRIX DTA TGA Temperature,C Fig. 11. DTA and TGA traces(heating rate 10-C/min) for the boehmite sol, showing the phase transformation ation test indicates that the ductile Ni interface was 10 R. Butler, E. G. and Ponton able to deflect the cracks created within the matrix sses.1995.10.1215 proving the presence of a weak interface. Thus, the Ponton, C. B. Ceram Transactions. vol. 8 composite produced in this work should show dam- merican Ceramic Society, Westerville, OH, 1998, pp age-tolerant' behaviour under the operation of crack deflection and fibre pull-out mechanisms. Further 12. Kaya, C. Trusty, P. A and Ponton, C B, in Better Cer- characterisation of the mechanical performance of mics Through Processing, eds J Binner and J. Yeomans, these composites, also at high-temperatures, is the 13. Kaya, C, Trusty, P. A. and Boccaccini, A.R., J.Eur focus of current research 14. Zhang, Z, Huang, Y. and Liang, Z, J. Am. Ceram. Soc cknowledgements-Professors M H. Loretto and I R are acknowledged for the provision of laboratory fa 15. Hirat Nishimoto, A and Ishihara. Y, Nippon Sera- tsu roi 992),108. sity of Birmingham, respectively. The authors would like to 16. Harbach, F and Nienburg,H,J.Eur. Ceram. Soc,1998 8,675 thank Dr Less Renny (Inco Speciality Powder Product, UK) 17. Boccaccini, A.R. and Trusty, P. A, J. Mater. Sci, 1998, for supplying the fibres. 18. Sarkar, P and Nicholson, P. S, J. Am. Ceram. Soc., 1996. REFERENCES 9(8),1987 1. Kilbride. I. P and Barker. A. J, Br. Ceram. Trans., 1994. 19. Kaya, C, PhD thesis, The University of Birmingham, 93(5),187 birmingham, UK 1999. Kumagai, M. and Messing. G. L.,J. Am. Ceram. Soc., 20. Kaya, C, Boccaccini, A. R and Chawla, K. K, J.Am Ceram.Soc,2000,83(8),1885 3. Kirk, R.E. and Othmer, D. F.(eds ) Encyclopedia of 21. Iston, T.J. Ponton, C.B., Marquis, P. M. and Butler,E. Chemical Technology, voL. 2. Wiley, New York, 1978, G, in Proceeding of the Third Euro Ceramics, eds P. pp.249 Duran and J. F. Fernandez, Madrid, Spain, vol. 1. 1993 ai,M. and Messing. G. L.,J. Am. Ceram. Soc., p.419 22. Trusty, P. A and Boccaccini, A R, Appl. Compos Mater. 5. McArdle, J. L. and Messing. G. L, J. Am. Ceram. Soc. 1986,69(7),C98 23. Boccaccini, A. R, Ovenstone, J. and Trusty, P. A, Appl. 6. Nicholson, P. S, Sarkar, P. and Huang, X, J. Mater. Sci. Compos Mater., 1997, 4(3), 145 1993,28 4. Morgan, P. E. D. and Marshall, D. B, J. Am. Cera. Soc. 7. Nicholson, P S, Sarkar, P and Huang, X. in Proceedings 1995,78(6,1553. Science and Technology of Zirconia VS, ed. S. P. S. 25. Kaya, C, Gu, X, Aldawery, I and Butler, E. G, submitted adwal. M. J. Bannister. R. H. J. Hannink, Technomic for publication, July 1999 993,p.503 6. Illston, T.J., MPhil thesis, The University of Birmingham, 8. Nicholson, P.S., Sarkar, P and Huang. X. J. An. Ceram. Birmingham, UK, 1995 oc,1992,75(10),2907 7. Prewo, K. M.J. Mater. Sci. 1982. 17. 3549 9. Kaya, C, Trusty, P. A and Ponton, C.B., Br. Ceram. 28. Marshall, D. B. and Evans, A. G.,J. Am. Ceram. Soc., Trans.,1998,81(10),48. 1986.68.225KAYA et al.: FABRICATION AND CHARACTERISATION OF ALUMINA CERAMIC MATRIX 1197 Fig. 11. DTA and TGA traces (heating rate 10°C/min) for the boehmite sol, showing the phase transformation temperatures and also the weight lost as a function of temperature. gation test indicates that the ductile Ni interface was able to deflect the cracks created within the matrix, proving the presence of a weak interface. Thus, the composite produced in this work should show ‘dam￾age-tolerant’ behaviour under the operation of crack deflection and fibre pull-out mechanisms. Further characterisation of the mechanical performance of these composites, also at high-temperatures, is the focus of current research. Acknowledgements—Professors M.H. Loretto and I.R. 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