张兵等：纯镍6平面热压缩变形行为及加工图 ·487· (a) I00μnm d 100μm 100μm 图11加工图中合理加工区内纯镍6的显微组织.(a)900℃，5s-1:(b)900℃，10s1:(c)1100℃，20s1:(d)1100℃，40s Fig.1 1 Microstructures of pure nickel N6 in the reasonable processing zone:(a)900℃，5s-l:(b)900℃，10s-l:(c)1I00℃，20s-l:(d) 1100℃，40s-1 [4]Huang T L,Chen HS,Liu Q.Grain orientation of large grain de- 1.98Cu-0.12Zr alloy during compression at elevated tempera- formation energy storage research the influence of industrial pure ture.Mater Sci Eng A,2014,608:63 nickel /The Second Session of the National Electron Back Scatter- [11]Zhou M,Lin Y C,Deng J,et al.Hot tensile deformation behav- ing Diffraction Technology and Application of the Test Results with iors and constitutive model of an Al-Zn-Mg-Cu alloy.Mater Electron Backscattered Diffraction (EBSD)Academic Conferences Des,2014,59:141 and the Sixth National Conference on Images of Materials Science [12]Wang M H,Huang L,Xian G C.Flow stress behavior of Cu-Ag and Technology.Baotou,2007:117 alloy under hot compression deformation.Chin J Rare Met, (黄天林，陈宏生，刘庆.晶粒取向对大品粒工业纯镍形变储 2013,37(5):695 能的影响研究/第二届全国背敢射电子衍射(EBSD)技术及 (王梦寒，黄龙，成国材.C山一Ag合金热压缩流变应力行为. 其应用学术会议暨第六届全国材料科学与图像科技学术会议 论文集.包头，2007：117) 稀有金属，2013,37(5)：695) 5]Peng HJ,Li D F,Guo Q M,et al.Processing map and tube hot [13]Lee B H,Reddy N S,Yeom JT,et al.Flow softening behavior extrusion of GH690 alloy.Chin J Rare Met,2012,36(2):184 during high temperature deformation of AZ31Mg alloy.J Mater (彭海健，李德富，郭青苗，等.CH690合金热加工图及管材 Process Techol,2007,187488:766 热挤压实验研究.稀有金属，2012,36(2)：184) [14]Li D F,Wu Z G,Guo S L,et al.Study on the processing map [6]Ju Q,Li D G,Liu G Q.The processing map of hot plastic de- of GH625 Ni-ased alloy deformed at high temperature.Rare Met formation of a 15Cr-25Ni-Fe base superalloy.Acta Metall Sin, Mater Eng,2012,41(6):1026 2006,42(2):218 (李德富，吾志岗，郭胜利，等。GH625镍基合金高温塑性 (鞠泉，李殿国，刘国权.15Cr-25NiFe基合金高温塑性变形 变形加工图研究.稀有金属材料与工程，2012,41(6)： 行为的加工图.金属学报，2006,42(2)：218) 1026) ]Cemri E,Evangelista E,MeQueen H J.Overview of the high tem- [15]Li J Q,Liu J,Cui Z S.Characterization of hot deformation be- perature substructure development in Al-Mg alloys.High Temp havior of extruded ZK60 magnesium alloy using 3D processing Mater Processes,1999,18:227 maps.Mater Des,2014,56:889 [8]Sellars C M,Tegart W J M.On the mechanism of hot deforma- 06 Zhang H B,Zhang K F,Lu Z,et al.Hot deformation behavior tion.Acta Metall,1996,14(9):1136 and processing map of a y-hardened nickel-based superalloy 9]Chen HQ,Deng W B.Hot Deformation behavior and microstruc- Mater Sci Eng A,2014,604:1 ture evolution of TCII titanium alloy with equiaxed structure.Chin 7] Zhao HZ,Xiao L,Ge P,et al.Hot deformation behavior and J Rare Met,2009,33(2):147 processing maps of Ti-1300 alloy.Mater Sci Eng A,2014,604: (陈慧琴，邓文斌.TC11钛合金等轴组织热变形行为与组织 111 演变.稀有金属，2009,33(2)：147) [18]Peng X N,Guo HZ,Shi Z F,et al.Study on the hot deforma- [0]Feng D.Zhang X M,Liu S D,et al.Constitutive equation and tion behavior of TC4-DT alloy with equiaxed+B starting struc- hot deformation behavior of homogenized Al-7.68Zn-2.12Mg- ture based on processing map.Mater Sci Eng A,2014,605:80张 兵等: 纯镍 N6 平面热压缩变形行为及加工图 图 11 加工图中合理加工区内纯镍 N6 的显微组织． ( a) 900 ℃，5 s － 1 ; ( b) 900 ℃，10 s － 1 ; ( c) 1100 ℃，20 s － 1 ; ( d) 1100 ℃，40 s － 1 Fig． 11 Microstructures of pure nickel N6 in the reasonable processing zone: ( a) 900 ℃，5 s － 1 ; ( b) 900 ℃，10 s － 1 ; ( c) 1100 ℃，20 s － 1 ; ( d) 1100 ℃，40 s － 1 ［4］ Huang T L，Chen H S，Liu Q． Grain orientation of large grain de￾formation energy storage research the influence of industrial pure nickel / / The Second Session of the National Electron Back Scatter￾ing Diffraction Technology and Application of the Test Ｒesults with Electron Backscattered Diffraction ( EBSD) Academic Conferences and the Sixth National Conference on Images of Materials Science and Technology． Baotou，2007: 117 ( 黄天林，陈宏生，刘庆． 晶粒取向对大晶粒工业纯镍形变储 能的影响研究 / / 第二届全国背散射电子衍射( EBSD) 技术及 其应用学术会议暨第六届全国材料科学与图像科技学术会议 论文集． 包头，2007: 117) ［5］ Peng H J，Li D F，Guo Q M，et al． Processing map and tube hot extrusion of GH690 alloy． Chin J Ｒare Met，2012，36( 2) : 184 ( 彭海健，李德富，郭青苗，等． GH690 合金热加工图及管材 热挤压实验研究． 稀有金属，2012，36( 2) : 184) ［6］ Ju Q，Li D G，Liu G Q． The processing map of hot plastic de￾formation of a 15Cr--25Ni--Fe base superalloy． Acta Metall Sin， 2006，42( 2) : 218 ( 鞠泉，李殿国，刘国权． 15Cr--25Ni--Fe 基合金高温塑性变形 行为的加工图． 金属学报，2006，42( 2) : 218) ［7］ Cerri E，Evangelista E，McQueen H J． Overview of the high tem￾perature substructure development in Al--Mg alloys． High Temp Mater Processes，1999，18: 227 ［8］ Sellars C M，Tegart W J M． On the mechanism of hot deforma￾tion． Acta Metall，1996，14( 9) : 1136 ［9］ Chen H Q，Deng W B． Hot Deformation behavior and microstruc￾ture evolution of TC11 titanium alloy with equiaxed structure． Chin J Ｒare Met，2009，33( 2) : 147 ( 陈慧琴，邓文斌． TC11 钛合金等轴组织热变形行为与组织 演变． 稀有金属，2009，33( 2) : 147) ［10］ Feng D，Zhang X M，Liu S D，et al． Constitutive equation and hot deformation behavior of homogenized Al--7. 68Zn--2. 12Mg-- 1. 98Cu--0. 12Zr alloy during compression at elevated tempera￾ture． Mater Sci Eng A，2014，608: 63 ［11］ Zhou M，Lin Y C，Deng J，et al． Hot tensile deformation behav￾iors and constitutive model of an Al--Zn--Mg--Cu alloy． Mater Des，2014，59: 141 ［12］ Wang M H，Huang L，Xian G C． Flow stress behavior of Cu--Ag alloy under hot compression deformation． Chin J Ｒare Met， 2013，37( 5) : 695 ( 王梦寒，黄龙，咸国材． Cu--Ag 合金热压缩流变应力行为． 稀有金属，2013，37( 5) : 695) ［13］ Lee B H，Ｒeddy N S，Yeom J T，et al． Flow softening behavior during high temperature deformation of AZ31Mg alloy． J Mater Process Techol，2007，187-188: 766 ［14］ Li D F，Wu Z G，Guo S L，et al． Study on the processing map of GH625 Ni-based alloy deformed at high temperature． Ｒare Met Mater Eng，2012，41( 6) : 1026 ( 李德富，吾志岗，郭胜利，等． GH625 镍基合金高温塑性 变形加工 图 研 究． 稀有金属材料与工程，2012，41 ( 6 ) : 1026) ［15］ Li J Q，Liu J，Cui Z S． Characterization of hot deformation be￾havior of extruded ZK60 magnesium alloy using 3D processing maps． Mater Des，2014，56: 889 ［16］ Zhang H B，Zhang K F，Lu Z，et al． Hot deformation behavior and processing map of a γ'-hardened nickel-based superalloy． Mater Sci Eng A，2014，604: 1 ［17］ Zhao H Z，Xiao L，Ge P，et al． Hot deformation behavior and processing maps of Ti--1300 alloy． Mater Sci Eng A，2014，604: 111 ［18］ Peng X N，Guo H Z，Shi Z F，et al． Study on the hot deforma￾tion behavior of TC4--DT alloy with equiaxed α + β starting struc￾ture based on processing map． Mater Sci Eng A，2014，605: 80 · 784 ·