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1996 L Zou et al. Journal of the eure eramic Society 23(2003)1987-1996 Youngs modulus of the Si3N4 matrix in the nitride/boron nitride ceramic. J. 4m. Ceram. Soc. 1996. 79 sandwiching sample due to its indirectly deter mination. However, this was solved by con 6. Kovar. Desiderio. Thouless. M. D. and Halloran. J W. Crack centrating all the deviations from the effecting deflection and propagation in layered silicon nitride/boron nitride factors upon the Youngs Modulus in Eqs. (5) 7. Kovar, D. King. B. H,Trice, R.W. and Halloran,J.w and (10). In this way, The e value was success Fibrous monolithic ceramics. J. Am. Ceram Soc. 1997 80 2471 fully adjusted to offset these influences. 8. Hai Guo, Yong Huang and Chang-an Wang, Preparation and Acknowledgements ng an Wang, Yong Huang. Qingfeng Zan, Hai Guo and Shengyou Cai, Biomimetic structure design-a possible approach The authors gratefully acknowledge Professor Z. D to change the brittleness of ceramics in nature. Materials science Guan for his much help in doing three-point bending Engineering C, 2000, 11, 9-12. tests; also this work was supported by National Natural 10. Charalambides. P. G. Lund. J. Evans. A. G R. M. A test specimen for determing the fracture resistance of Science Foundation of China(No. 59632090) bimaterial interfaces. J. Appl. Mech, 1989, 56. 77-82 I1. Phillips, A.J. Clegg, w.J. and Clyne, T.W., Fracture behavior of ceramic laminates in bending-lI. Comparison of model pre- References dictions with e data. Acta Metall. Mater. 1993. 41 819-827 12. Phillips, A.J., Clegg, w.J. and Clyne, T.w Fracture behavior 1. Clegg. W.J., Kendall. K, Alford, N. M., Birchall, D. and But- hates in bending-1. Modelling of crack propa- s. Nature. 1990 gation. Acta Metall. Mater., 1993, 41. 805-817 13. Clyne, T. w. and Phillips, A. J, Interfacial control and macro- 2. Baskaran, S, Nunn, S. D, Popovic, Dragan and Halloran, J. w scopic failure in long-fiber-reinforced and laminated inorganic Fibrous monolithic ceramics: 1. fabrication. microstructure composites. Composites Sci. Tech, 1994, 51, 271-282 and indentation behavior. J. Am. Ceram Soc., 1993, 76, 2209- 14. Cao, H. C. and Evans, A. G, An experimental study of the fracture resistance of bimaterial interfaces. Mechanics of materi. neolithic ceramics als,1989,7,295-304 Il, flexural strength and fracture bhavior of the slicon carbide/ 15. Linhua Zou, Interfacial toughness measurement and characteriza- graphite system. J. Am. Ceram. Soc., 1993, 76, 2217-2224. tion for Si3N4/ BN composites. Report of Postdoctoral Research, 4. Baskaran. S. and Halloran. J. W. Fibrous monolithic ceramics: Tsinghua University, Beijing, 2002. Ill, mechanical properties and oxidation beha 16. Trice. R. w. and Halloran, J W.. Influence of microstructure and carbide/ boron nitride system. J. Am. Ceram. Soc., 1994, 77 mperature on the interfacial fracture energy of silicon nitride/ boron nitride fibrous monolithic ceramics. Am. Ceran. Soc 5. Liu, H. and Hsu. S M, Fracture behavior of multilayer silicon 1999,82,2502-2508Young’s modulus of the Si3N4 matrix in the sandwiching sample due to its indirectly deter￾mination. However,this was solved by con￾centrating all the deviations from the effecting factors upon the Young’s Modulus in Eqs. (5) and (10). In this way,The E value was success￾fully adjusted to offset these influences. Acknowledgements The authors gratefully acknowledge Professor Z. D. Guan for his much help in doing three-point bending tests; also this work was supported by National Natural Science Foundation of China (No.59632090). References 1. Clegg,W. J.,Kendall,K.,Alford,N. M.,Birchall,D. and But￾ton,T. W.,A simple way to make tough ceramics. Nature,1990, 347,445–447. 2. Baskaran,S.,Nunn,S. D.,Popovic,Dragan and Halloran,J. W., Fibrous monolithic ceramics: I,fabrication,microstructure, and indentation behavior. J. Am. Ceram. Soc.,1993, 76,2209– 2216. 3. Baskaran,S. and Halloran,J. W.,Fibrous monolithic ceramics: II,flexural strength and fracture bhavior of the slicon carbide/ graphite system. J. Am. Ceram. Soc.,1993, 76,2217–2224. 4. Baskaran,S. and Halloran,J. W.,Fibrous monolithic ceramics: III,mechanical properties and oxidation behavior of the silicon carbide/boron nitride system. J. Am. Ceram. Soc.,1994, 77, 1249–1255. 5. Liu,H. and Hsu,S. M.,Fracture behavior of multilayer silicon nitride/boron nitride ceramic. J. Am. Ceram. Soc.,1996, 79, 2452–2457. 6. Kovar,Desiderio,Thouless,M. D. and Halloran,J.W.,Crack deflection and propagation in layered silicon nitride/boron nitride ceramics. J. Am. Ceram. Soc.,1998, 81,1004–1012. 7. Kovar,D.,King,B. H.,Trice,R. W. and Halloran,J. W., Fibrous monolithic ceramics. J. Am. Ceram. Soc.,1997, 80,2471– 2487. 8. Hai Guo,Yong Huang and Chang-an Wang,Preparation and properties of fibrous monolithic ceramic by in-situ synthesizing. J. Mater. Sci.,1999, 34,2455–2459. 9. Chang-an Wang,Yong Huang,Qingfeng Zan,Hai Guo and Shengyou Cai,Biomimetic structure design—a possible approach to change the brittleness of ceramics in nature. Materials Science & Engineering C,2000, 11,9–12. 10. Charalambides,P. G.,Lund,J.,Evans,A. G. and McMeeking, R. M.,A test specimen for determing the fracture resistance of bimaterial internfaces. J. Appl. Mech,1989, 56,77–82. 11. Phillips,A. J.,Clegg,W. J. and Clyne,T. W.,Fracture behavior of ceramic laminates in bending—II. Comparison of model pre￾dictions with experimental data. Acta Metall. Mater.,1993, 41, 819–827. 12. Phillips,A. J.,Clegg,W. J. and Clyne,T. W.,Fracture behavior of ceramic laminates in bending—I. Modelling of crack propa￾gation. Acta Metall. Mater.,1993, 41,805–817. 13. Clyne,T. W. and Phillips,A. J.,Interfacial control and macro￾scopic failure in long-fiber-reinforced and laminated inorganic composites. Composites Sci. Tech.,1994, 51,271–282. 14. Cao,H. C. and Evans,A. G.,An experimental study of the fracture resistance of bimaterial interfaces. Mechanics of Materi￾als,1989, 7,295–304. 15. Linhua Zou, Interfacial toughness measurement and characteriza￾tion for Si3N4/BN composites. Report of Postdoctoral Research, Tsinghua University,Beijing,2002. 16. Trice,R.W. and Halloran,J.W.,Influence of microstructure and temperature on the interfacial fracture energy of silicon nitride/ boron nitride fibrous monolithic ceramics. J. Am. Ceram. Soc., 1999, 82,2502–2508. 1996 L. Zou et al. / Journal of the European Ceramic Society 23 (2003) 1987–1996
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