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·210· 工程科学学报,第37卷,第2期 置,容易产生裂纹,在Mg1.5Zn0.9Ce合金中产生了 in high strength wrought magnesium alloys.Scripta Metall Mater, 较大的第二相粒子,虽然其(0002)极图的最大强度仅 1994,31(2):111 为3.4,但在杯突实验中其埃里克森杯突值只能达到 [8]Sanjari M,Farzadfar S F,Sakai T,et al.Microstructure and tex- ture evolution of Mg3Zn3Ce magnesium alloys sheets and associat- 3.84. ed restoration mechanisms during annealing.Mater Sci Eng A, 3结论 2013,561:191 ]Lu CJ.Sudy on Rolling Process and Properties of AZ31 Magnesi- 研究了变形Mg一l.5Zn一xCe合金的织构及室温成 um Alloy Sheet with Fine Grain DDissertation ]Beijing:Universi- 形性能.结果表明:在Mg-1.5Zn合金中添加0.2%的 ty of Science and Technology Beijing,2012 (陆春洁.细品AZ31镁合金板材的轧制工艺及性能研究[学 Ce元素后,可以有效降低合金的基面织构强度,使c 位论文].北京:北京科技大学,2012) 轴由法向向横向偏移,提高了合金的室温成形性能:然 [10]Akhtar A,Teghtsoonian E.Solid solution strengthening of mag- 而,当在Mg-1.5Zm合金中添加过量的Ce会使织构强 nesium single crystals:I.Alloying behaviour in basal slip.Acta 度增强,生成粗大的MgZnCe第二相粒子,导致合金的 Metall,1969,17(11):1339 室温成形性能变差 [11]Chino Y,Kado M,Mabuchi M.Compressive deformation behav- ior at room temperature-773 K in Mg-0.2 mass%(0.035at.% Ce alloy.Acta Mater,2008,56(3):387 参考文献 [12] Stanford N,Barnett M R.The origin of "rare earth"texture de- [1]Li Y D,Chen T J,Ma Y,et al.Effect of rare earth 0.5%addi- velopment in extruded Mg-based alloys and its effect on tensile tion on semi-solid microstructural evolution of AZ91D alloy.Chin ductility.Mater Sci Eng A,2008,496 (12):399 JNonferrous Met,2007,17(2)320 [13]Chino Y,Huang X S,Suzuki K,et al.Influence of Zn concen- ]Yoshinaga H,Horiuchi R.Deformation mechanisms in magnesium tration on stretch formability at room temperature of Mg-Zn-Ce single crystals compressed in the direction parallel to hexagonal ax- alloy.Mater Sci Eng A,2010,528(2)566 is.Trans JIM,1963,4(1):1 [14]Huang X S,Suzuki K,Watazu A,et al.Improvement of form- 3]Mukai T,Yamanoi M,Watanabe H,et al.Ductility enhancement ability of Mg-Al-Zn alloy sheet at low temperatures using differ- in A231 magnesium alloy by controlling its grain structure.Scripta ential speed rolling.J Alloys Compd,2009,470(12):263 Mater,2001,45(1):89 [15]Chino Y,Sassa K.Kamiva A,et al.Influence of rolling routes 4]Chino Y,Kado M,Mabuchi M.Enhancement of tensile ductility on press formability of a rolled A731 Mg alloy sheet.Mater and stretch formability of magnesium by addition of 0.2 wt% Trans,2006,47(10):2555 (0.035at%)Ce.Mater Sci Eng A,2008,494(12):343 [16]Chino Y,Mabuchi M.Enhanced stretch formability of Mg-Al- [5]Wu D.Chen R S,Han E H.Excellent room-emperature ductility Zn alloy sheets rolled at high temperature (723 K).Scripta Ma- and formability of rolled Mg-Gd-Zn alloy sheets.J Alloys Compd, ter,2009,60(6):447 2011,509(6):2856 07] Yan H.Chen R S,Han E H.Room-temperature ductility and [6]Yan H,Chen R S,Han E H.A comparative study of texture and anisotropy of two rolled Mg-Zn-Gd alloys.Mater Sci Eng A, ductility of Mg-1.2Zn-0.8Gd alloy fabricated by rolling and e- 2010,527(15):3317 qual channel angular extrusion.Mater Charact,2011,62(3): [18]Chino Y,Sassa K.Mabuchib M.Texture and stretch formability 321 of a rolled Mg-Zn alloy containing dilute content of Y.Mater Sci 7]Ball E A,Prangnell P B.Tensile-compressive yield asymmetries EngA,2009,513514:394工程科学学报,第 37 卷,第 2 期 置,容易产生裂纹,在 Mg--1. 5Zn--0. 9Ce 合金中产生了 较大的第二相粒子,虽然其( 0002) 极图的最大强度仅 为 3. 4,但在杯突实验中其埃里克森杯突值只能达到 3. 84. 3 结论 研究了变形 Mg--1. 5Zn--xCe 合金的织构及室温成 形性能. 结果表明: 在 Mg--1. 5Zn 合金中添加 0. 2% 的 Ce 元素后,可以有效降低合金的基面织构强度,使 c 轴由法向向横向偏移,提高了合金的室温成形性能; 然 而,当在 Mg--1. 5Zn 合金中添加过量的 Ce 会使织构强 度增强,生成粗大的 MgZnCe 第二相粒子,导致合金的 室温成形性能变差. 参 考 文 献 [1] Li Y D,Chen T J,Ma Y,et al. Effect of rare earth 0. 5% addi￾tion on semi-solid microstructural evolution of AZ91D alloy. Chin J Nonferrous Met,2007,17( 2) : 320 [2] Yoshinaga H,Horiuchi R. Deformation mechanisms in magnesium single crystals compressed in the direction parallel to hexagonal ax￾is. Trans JIM,1963,4( 1) : 1 [3] Mukai T,Yamanoi M,Watanabe H,et al. Ductility enhancement in AZ31 magnesium alloy by controlling its grain structure. Scripta Mater,2001,45( 1) : 89 [4] Chino Y,Kado M,Mabuchi M. Enhancement of tensile ductility and stretch formability of magnesium by addition of 0. 2 wt% ( 0. 035 at% ) Ce. Mater Sci Eng A,2008,494( 1-2) : 343 [5] Wu D,Chen R S,Han E H. Excellent room-temperature ductility and formability of rolled Mg--Gd--Zn alloy sheets. J Alloys Compd, 2011,509( 6) : 2856 [6] Yan H,Chen R S,Han E H. A comparative study of texture and ductility of Mg--1. 2Zn--0. 8Gd alloy fabricated by rolling and e￾qual channel angular extrusion. Mater Charact,2011,62 ( 3 ) : 321 [7] Ball E A,Prangnell P B. Tensile-compressive yield asymmetries in high strength wrought magnesium alloys. Scripta Metall Mater, 1994,31( 2) : 111 [8] Sanjari M,Farzadfar S F,Sakai T,et al. Microstructure and tex￾ture evolution of Mg3Zn3Ce magnesium alloys sheets and associat￾ed restoration mechanisms during annealing. Mater Sci Eng A, 2013,561: 191 [9] Lu C J. Study on Rolling Process and Properties of AZ31 Magnesi￾um Alloy Sheet with Fine Grain[Dissertation〗. Beijing: Universi￾ty of Science and Technology Beijing,2012 ( 陆春洁. 细晶 AZ31 镁合金板材的轧制工艺及性能研究[学 位论文]. 北京: 北京科技大学,2012) [10] Akhtar A,Teghtsoonian E. Solid solution strengthening of mag￾nesium single crystals: I. Alloying behaviour in basal slip. Acta Metall,1969,17( 11) : 1339 [11] Chino Y,Kado M,Mabuchi M. Compressive deformation behav￾ior at room temperature--773 K in Mg--0. 2 mass% ( 0. 035at. % ) Ce alloy. Acta Mater,2008,56( 3) : 387 [12] Stanford N,Barnett M R. The origin of“rare earth”texture de￾velopment in extruded Mg-based alloys and its effect on tensile ductility. Mater Sci Eng A,2008,496 ( 1-2) : 399 [13] Chino Y,Huang X S,Suzuki K,et al. Influence of Zn concen￾tration on stretch formability at room temperature of Mg--Zn--Ce alloy. Mater Sci Eng A,2010,528( 2) : 566 [14] Huang X S,Suzuki K,Watazu A,et al. Improvement of form￾ability of Mg--Al--Zn alloy sheet at low temperatures using differ￾ential speed rolling. J Alloys Compd,2009,470( 1-2) : 263 [15] Chino Y,Sassa K,Kamiya A,et al. Influence of rolling routes on press formability of a rolled AZ31 Mg alloy sheet. Mater Trans,2006,47( 10) : 2555 [16] Chino Y,Mabuchi M. Enhanced stretch formability of Mg--Al-- Zn alloy sheets rolled at high temperature ( 723 K) . Scripta Ma￾ter,2009,60( 6) : 447 [17] Yan H,Chen R S,Han E H. Room-temperature ductility and anisotropy of two rolled Mg--Zn--Gd alloys. Mater Sci Eng A, 2010,527( 15) : 3317 [18] Chino Y,Sassa K,Mabuchib M. Texture and stretch formability of a rolled Mg--Zn alloy containing dilute content of Y. Mater Sci Eng A,2009,513-514: 394 · 012 ·
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