生物大分子波谱学原理 吴季辉 CCONH-TOCSY Basic triple resonance experiments:(H)CCCONH TOCSY 3D (HCC(CO)NH Haliph.->Caliph-(t1)->Ca.->C'->N(t2)->HN(t3) 3 S3 S2 S1 T 2 2 DIPSI-2(x) al .2S33 15N isu GARP ,2ST, 21Ty 13C 222Ds-2 2S3】 BSP 2SSzy KGz Gz K=+/-10V=+/-y91=y;92=2(x,2(-x)+TPPI(t53=x5 94=Xg5=x,-X9e=X,2(-x,k △'-3.6ms,A"=2.4ms,△=5.4ms,t=13.5ms,=3.4ms,=4.5ms.CCONH -TOCSY 生物大分子波谱学原理 吴季辉