生物大分子波谱学原理 吴季梅 HCONH-TOCSY Basic triple resonance experiments:H(CC)CONH TOCSY 3D H(CC)(CO)NH ti,t H 2 2DIPSI-22) DIPs-22 △j, 15N 凯 GARP 13C BSP t2 DIPSI-2() BSP Gz Gz K=+-10Ψ=+/-y;01=y,-y+TPPI5◆2=x;93=x;◆4=x; 05=2(x),2(-x596=X07=x;中e=X,2(-x),x △=5.4ms,t=13.5ms,t1=6ms,t2=12ms,=3.4ms,n=4.5ms. using homo-and heteronuclear TOCSY transfer ·→time-saving by simultaneous1H-13℃and13C-13℃transfer HCONH-TOCSY 生物大分子波谱学原理 吴季辉