.1288· 北京科技大学学报 第35卷 [17]Liu M S,Li H G,Sun P M,et al.Study on mechani- (王晓辉，郑诗礼，徐红彬，等.ICP-AES法测定难分解钽 cal activated decomposition with soda solution of scheelite 铌矿渣中多种金属元素.光谱学与光谱分析，2009,29(3)： middle concentrate.J Cent South Inst Min Metall,1994 805) 25(3):321 [22]Zhou K G,Tokuda M.Study on solubility of Nb2Os in (刘茂盛，李洪桂，孙培梅，等。机械活化苏打溶液分解白钨 KOH solution and alkali leaching of niobite.J Cent South 中矿试验研究.中南矿治学院学报，1994,25(3)：321) Univ TechnoL 2000,7(4):171 [18]Zhou H M,Yi D Q,Zhang Y,et al.The dissolution be- [23]Zhao Z W,Sun P M,Li Y J,et al.Some problems con- havior of Nb2Os,Ta2Os and their mixture in highly con- cerning the understanding of enhancing metallurgical pro- centrated KOH solution.Hydrometallurgy,2005,80(1/2) cesses by mechanochemical methods.J Cent South Univ 126 Technol,1995,26(6):757 (19]Wang X H,Zheng S L,Xu H B,et al.Dissolution behav- (超中伟，孙培梅，李运姣，等.机械活化强化治金反应的几 iors of Ta2Os,Nb2Os and their mixture in KOH and H2O 个问题.中南工业大学学报，1995,26(06)：757) system.Trans Nonferrous Met Soc China,2010,20(10): [24 Fah C P,Wang J.Effect of high-energy mechanical acti- 2006 vation on the microstructure and electrical properties of [20]Guo Q W,Wang Z X.Modern Niobium-Tantalum Metal- ZnO-based varistors.Solid State Ionics,2000,132(1/2): lurgy.Ist Ed.Beijing:Metallurgical Industry Press,2009 107 (郭青蔚，王肇信.现代铌钽治金.1版.北京：治金工业出 [25]Chen X,Li C H.Crystallite size and lattice distortion of 版社，2009) TiC from X-ray diffraction line profile analysis.Cemented [21]Wang X H,Zheng S L,Xu H B,et al.Analysis of metal- Carbide,.2009,26(2):106 lic elements in refractory tantalum-niobium slag by ICP- (陈霞，李晨辉.用XRD线形分析法表征TC粉体中的镶 AES.Spectrosc Spectral Anal 2009,29(3):805 嵌尺寸与晶格畸变.硬质合金，2009,26(2)：106)· 1288 · 北 京 科 技 大 学 学 报 第 35 卷 [17] Liu M S, Li H G, Sun P M, et al. Study on mechani￾cal activated decomposition with soda solution of scheelite middle concentrate. J Cent South Inst Min Metall, 1994, 25(3): 321 (刘茂盛, 李洪桂, 孙培梅, 等. 机械活化苏打溶液分解白钨 中矿试验研究. 中南矿冶学院学报, 1994, 25(3): 321) [18] Zhou H M, Yi D Q, Zhang Y, et al. The dissolution be￾havior of Nb2O5, Ta2O5 and their mixture in highly con￾centrated KOH solution. Hydrometallurgy, 2005, 80(1/2): 126 [19] Wang X H, Zheng S L, Xu H B, et al. Dissolution behav￾iors of Ta2O5, Nb2O5 and their mixture in KOH and H2O system. Trans Nonferrous Met Soc China, 2010, 20(10): 2006 [20] Guo Q W, Wang Z X. Modern Niobium-Tantalum Metal￾lurgy. 1st Ed. Beijing: Metallurgical Industry Press, 2009 (郭青蔚, 王肇信. 现代铌钽冶金. 1 版. 北京: 冶金工业出 版社, 2009) [21] Wang X H, Zheng S L, Xu H B, et al. Analysis of metal￾lic elements in refractory tantalum-niobium slag by ICP￾AES. Spectrosc Spectral Anal, 2009, 29(3): 805 (王晓辉, 郑诗礼, 徐红彬, 等. ICP-AES 法测定难分解钽 铌矿渣中多种金属元素. 光谱学与光谱分析, 2009, 29(3): 805) [22] Zhou K G, Tokuda M. Study on solubility of Nb2O5 in KOH solution and alkali leaching of niobite. J Cent South Univ Technol, 2000, 7(4): 171 [23] Zhao Z W, Sun P M, Li Y J, et al. Some problems con￾cerning the understanding of enhancing metallurgical pro￾cesses by mechanochemical methods. J Cent South Univ Technol, 1995, 26(6): 757 (赵中伟, 孙培梅, 李运姣, 等. 机械活化强化冶金反应的几 个问题. 中南工业大学学报, 1995, 26(06): 757) [24] Fah C P, Wang J. Effect of high-energy mechanical acti￾vation on the microstructure and electrical properties of ZnO-based varistors. Solid State Ionics, 2000, 132(1/2): 107 [25] Chen X, Li C H. Crystallite size and lattice distortion of TiC from X-ray diffraction line profile analysis. Cemented Carbide, 2009, 26(2): 106 (陈霞, 李晨辉. 用 XRD 线形分析法表征 TiC 粉体中的镶 嵌尺寸与晶格畸变. 硬质合金, 2009, 26(2): 106)