第36卷第5期 北京科技大学学报 Vol.36 No.5 2014年5月 Journal of University of Science and Technology Beijing May 2014 430不锈钢冷轧板高温退火过程中再结晶织构的定量 分析 王乃帅,张雄”,温治),豆瑞锋区,李志强” 1)北京科技大学机械工程学院,北京1000832)北京科技大学治金工业节能减排北京市重点实验室,北京100083 ☒通信作者,E-mail:douruifeng@(126.com 摘要在750,800.825和850℃温度下,利用Gleeble1500热模拟试验机对430不锈钢冷轧薄板的等温退火过程进行了详细 的实验研究,分析了退火过程中再结晶织构和组织的变化规律,并对关键织构体积分数的演变进行了定量分析.结果发现:随 着退火过程的进行,α《取向线上的织构强度逐渐减弱,而Y取向线上的织构强度则略有加强,并保持在较高的值:再结晶过程 中,{111}和{112}<110>织构的体积分数逐渐降低,而{100}和随机取向晶粒的体积分数逐渐增加.定量分析表明,退火温 度越低,完全再结晶后材料内部关键织构的体积分数越偏离冷轧态.最后,针对{111}、{112}〈110>、{100}和随机取向织构 的体积分数在再结晶过程中的演变规律,建立了MAK型再结晶织构演变动力学模型. 关键词不锈钢:等温退火;再结品;织构 分类号TG142.71 Quantitative analysis of the recrystallized textures of cold-rolled 430 stainless steel during high-temperature annealing WANG Nai-shuai,ZHANG Xiong,WEN Zhi,DOU Rui-feng,LI Zhi-qiang) 1)School of Mechanical Engineering,University of Science and Technology Beijing,Beijing 100083,China 2)Beijing Key Laboratory for Energy Saving and Emission Reduction of Metallurgical Industry,University of Science and Technology Beijing,Beijing 100083,China Corresponding author,E-mail:douruifeng@126.com ABSTRACT Variations in the recrystallized texture and microstructure of cold-rolled 430 stainless steel during isothermal annealing were investigated on a Gleeble-1500 thermal-mechanic simulator at 750,800,825 and 850C,and the evolution of main textures was analyzed quantitatively.As annealing proceeds,the intensity of a-fiber orientation components decreases,but the intensity of y-fiber components increases slightly and maintains at a higher value.The volume fraction of (111)and (112)(110>decreases as recrystal- lization proceeds,while the volume fraction of (100}and random orientation textures increases.Compared with the cold-rolled state,it is observed that the volume fraction of main textures has greater changes in annealing at low temperature than at high temperature. Finally,variations in the volume fraction of (111},(112)(110,(100}and random orientation textures during recrystallization were described by a JMAK kinetics model. KEY WORDS stainless steel:isothermal annealing:recrystallization:textures 430不锈钢属于最早开发的铁素体不锈钢钢种替了奥氏体不锈钢·习.为了满足这些领域对薄板 之一,由于不含镍且有很强的抗氯化物应力腐蚀能 材料性能的要求,需要保证430薄板有很好的深冲 力等优势,其在家电和汽车领域已经很大程度上代 性能以及成型性能.冷轧板的再结晶织构是影响其 收稿日期:20130303 基金项目:中央高校基本科研业务费专项资金资助项目(FRF一AS-10O05B) DOI:10.13374/j.issn1001-053x.2014.05.010:http://journals.ustb.edu.cn第 36 卷 第 5 期 2014 年 5 月 北京科技大学学报 Journal of University of Science and Technology Beijing Vol. 36 No. 5 May 2014 430 不锈钢冷轧板高温退火过程中再结晶织构的定量 分析 王乃帅1) ,张 雄1) ,温 治2) ,豆瑞锋1) ,李志强1) 1) 北京科技大学机械工程学院,北京 100083 2) 北京科技大学冶金工业节能减排北京市重点实验室,北京 100083 通信作者,E-mail: douruifeng@ 126. com 摘 要 在 750、800、825 和 850 ℃温度下,利用 Gleeble1500 热模拟试验机对 430 不锈钢冷轧薄板的等温退火过程进行了详细 的实验研究,分析了退火过程中再结晶织构和组织的变化规律,并对关键织构体积分数的演变进行了定量分析. 结果发现: 随 着退火过程的进行,α 取向线上的织构强度逐渐减弱,而 γ 取向线上的织构强度则略有加强,并保持在较高的值; 再结晶过程 中,{ 111} 和{ 112} < 110 > 织构的体积分数逐渐降低,而{ 100} 和随机取向晶粒的体积分数逐渐增加. 定量分析表明,退火温 度越低,完全再结晶后材料内部关键织构的体积分数越偏离冷轧态. 最后,针对{ 111} 、{ 112} ?110 > 、{ 100} 和随机取向织构 的体积分数在再结晶过程中的演变规律,建立了 JMAK 型再结晶织构演变动力学模型. 关键词 不锈钢; 等温退火; 再结晶; 织构 分类号 TG 142. 71 Quantitative analysis of the recrystallized textures of cold-rolled 430 stainless steel during high-temperature annealing WANG Nai-shuai1) ,ZHANG Xiong1) ,WEN Zhi2) ,DOU Rui-feng1) ,LI Zhi-qiang1) 1) School of Mechanical Engineering,University of Science and Technology Beijing,Beijing 100083,China 2) Beijing Key Laboratory for Energy Saving and Emission Reduction of Metallurgical Industry,University of Science and Technology Beijing,Beijing 100083,China Corresponding author,E-mail: douruifeng@ 126. com ABSTRACT Variations in the recrystallized texture and microstructure of cold-rolled 430 stainless steel during isothermal annealing were investigated on a Gleeble-1500 thermal-mechanic simulator at 750,800,825 and 850 ℃,and the evolution of main textures was analyzed quantitatively. As annealing proceeds,the intensity of α-fiber orientation components decreases,but the intensity of γ-fiber components increases slightly and maintains at a higher value. The volume fraction of { 111} and { 112} ?110 > decreases as recrystallization proceeds,while the volume fraction of { 100} and random orientation textures increases. Compared with the cold-rolled state,it is observed that the volume fraction of main textures has greater changes in annealing at low temperature than at high temperature. Finally,variations in the volume fraction of { 111} ,{ 112} ?110? ,{ 100} and random orientation textures during recrystallization were described by a JMAK kinetics model. KEY WORDS stainless steel; isothermal annealing; recrystallization; textures 收稿日期: 2013--03--03 基金项目: 中央高校基本科研业务费专项资金资助项目( FRF--AS--10--005B) DOI: 10. 13374 /j. issn1001--053x. 2014. 05. 010; http: / /journals. ustb. edu. cn 430 不锈钢属于最早开发的铁素体不锈钢钢种 之一,由于不含镍且有很强的抗氯化物应力腐蚀能 力等优势,其在家电和汽车领域已经很大程度上代 替了奥氏体不锈钢[1--2]. 为了满足这些领域对薄板 材料性能的要求,需要保证 430 薄板有很好的深冲 性能以及成型性能. 冷轧板的再结晶织构是影响其