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.1474. 工程科学学报,第40卷,第12期 lurgy in China.Chin J Rare Met,2003,27(1):18 34(1):36 (肖连生,张启修,李青刚.我国钨治炼技术的新进展.稀有 (戴艳阳,钟海云,李荐,等.钨渣中有价金属综合回收工 金属.2003,27(1):18) 艺.中南工业大学学报(自然科学版),2003,34(1):36) [3] Medvedev A S,Aleksandrov P V,Razykov B Z,et al.Prospects [14]Wang JJ,Wang X H,Zhang Y,et al.Comprehensive recovery for involvement of low-grade molybdenum and tungsten concen- of tantalum and niobium from tantalum-niobium residue.Chin J trates in metallurgical processing.Metallurgist,2013,57(34): Rare Met,2015,39(3):251 261 (汪加军,王晓辉,张盈,等.含钽铌废渣中钽铌资源的综合 [4]Zhao Z W.Tungsten Metallurgy:Fundamentals and Applications. 回收工艺研究.稀有金属,2015,39(3):251) Beijing:Tsinghua University Press,2013 [15]Yang X L,Wang X H,Xiang S B,et al.Enrichment of tantalum (赵中伟.钨治炼的理论与应用.北京:清华大学出版社, and niobium from tungsten residue by hydrochloric acid method- 2013) he.Chin J Nonferrous Met,2013,23(3):873 [5]Dai YY.Study on the Ne Cleaner Process of Comprehensice Re- (杨秀丽,王晓辉,向仕彪,等.盐酸法富集钨渣中的钽和 covery of Valuble Metals from Tungsten Residues Dissertation]. 铌.中国有色金属学报,2013,23(3):873) Changsha:Central South University,2013 [16]Xiang S B,Huang B,Wang X H,et al.Research on recovery of (戴艳阳.钨渣中有价金属综合回收新清洁工艺研究[学位论 tantalum and niobium from tungsten residue by acid method. 文].长沙:中南大学,2013) Nonferrous Met Eng Res,2012,33(2):5 [6]Wang X H,Xiang S B,Zheng S L,et al.A method for extracting (向仕彪,黄波,王晓辉,等.从废钨渣中酸法回收钽铌的研 potassium tantalum,niobium and potassium fluosilicate from tung 究.有色冶金设计与研究,2012,33(2):5) sten smelting slag:China Patent,CN201110240762.5.2013-03- [17]Wu B,Shang H.Wen J K.Leaching of niobium from low-grade 06 refractory tantalum-niobium bearing minerals.Chin Rare Met, (王晓辉,向仕彪,郑诗礼,等。一种从钨冶炼渣中提取钽、铌 2013,37(5):791 并联产氟硅酸钾的方法:中国专利,CN201110240762.5. (武彪,尚鹤,温建康.低品位难处理钽铌矿中铌的浸出试 2013-03-06) 验研究.稀有金属,2013,37(5):791) [7]Luo X P,Liu B L,Tang M K.Experimental investigation of com- [18]Nete M,Purcell W,Nel J T.Non-fluoride dissolution of tanta- plex recovery of valuable minerals components containing in the lum and niobium oxides and their separation using ion exchange. residue abandoned in wet-metallurgical process of wolframite ores. Hydrometallurgy,2017,173:192 China Tungsten Ind,2005,20(3):24 [19]Deblonde G J P,Weigel V,Bellier Q,et al.Selective recovery (罗仙平,刘北林,唐敏康.从钨治炼渣中综合回收有价金属 of niobium and tantalum from low-grade concentrates using a sim- 的试验研究.中国钨业,2005,20(3):24) ple and fluoride-free process.Sep Purif Technol,2016,162:180 [8]Liang W D.Application of two stage autoclave process for higher [20]Kabangu M J,Crouse P L.Separation of niobium and tantalum tungsten metallurgical recovery //9th National Hard Alloy Aca- from Mozambican tantalite by ammonium bifluoride digestion and demic Conference.Chengdu,2006:117 octanol solvent extraction.Hydrometallurgy,2012,129-130: (梁卫东.二次压煮工艺提高钨治炼金属回收率的应用/第 151 九次全国硬质合金学术会议.成都,2006:117) [21]Wang WW,Pranolo Y,Cheng C Y.Recovery of scandium from [9]Du Y.Research on Recovery of Tungsten from Enriched Tungsten synthetic red mud leach solutions by solvent extraction with Residue Dissertation ]Xi'an:Xi'an University of Architecture D2EHPA.Sep Purif Technol,2013,108:96 and Technology,2014 [22]Ding C,Wang X H,He C R,et al.Sulfuric acid leaching of (杜阳.富钨渣中回收钨的研究[学位论文].西安:西安建筑 scandium from black tungsten ore slag and depression leaching of 科技大学,2014) iron by carphosiderite method.Chin J Process Eng,2014,14 [10]Wu Y Q,Wu X,Ma G.Tungsten recovery from the residue after (6):907 acid leaching of superalloy.Min Metall Eng,2014,34(6):101 (丁冲,王晓辉,何超然,等.黑钨渣硫酸浸钪及浸出过程中 (吴永谦,吴贤,马光.从某高温合金酸浸渣中回收钨的研 草黄铁矾法抑制铁浸出.过程工程学报,2014,14(6):907) 究.矿冶工程,2014,34(6):101) [23] Liang H L,Luo D M,Liu C,et al.Leaching of scandium oxide [11]Yang S H,Wang J.Xie B R,et al.Treatment process of low- from tungsten slag.Hydrometall China,2015,34(2):114 grade tungsten slag.Nonferrous Met Sci Eng,2015,6(6):29 (梁焕龙,罗东明,刘晨,等.从钨渣中浸出氧化钪的试验研 (杨少华,王君,谢宝如,等.低品位钨渣处理工艺.有色金 究.湿法治金,2015,34(2):114) 属科学与工程,2015,6(6):29) [24]Wang WW,Pranolo Y,Cheng C Y.Metallurgical processes for [12]Chen HZ.Recovering tungsten-fermanganum from tungsten slag. scandium recovery from various resources:a review.Hydrometal- China Mater Recycl,1992(8):42 lrgy,2011,108(1-2):100 (陈洪泽.从钨渣中回收钨钪铁锰.中国物资再生,1992 [25]Vanderpool C D.Huang Y X.Recovery of tungsten ferroscandi- (8):42) um and manganese from tungsten containing materials.Conser [13]Dai YY,Zhong H Y,Li J,et al.Valuable metals'recovery from Utiliz Miner Resour,1989(1):42 tungsten residue.J Cent South Univ Technology Nat Sci,2003, (Clarence D Vanderpool,黄永校.从含钨物料中回收钨钪铁工程科学学报,第 40 卷,第 12 期 lurgy in China. Chin J Rare Met, 2003, 27(1): 18 (肖连生, 张启修, 李青刚. 我国钨冶炼技术的新进展. 稀有 金属, 2003, 27(1): 18) [3] Medvedev A S, Aleksandrov P V, Razykov B Z, et al. Prospects for involvement of low鄄grade molybdenum and tungsten concen鄄 trates in metallurgical processing. Metallurgist, 2013, 57 (3鄄4): 261 [4] Zhao Z W. Tungsten Metallurgy: Fundamentals and Applications. Beijing: Tsinghua University Press, 2013 (赵中伟. 钨冶炼的理论与应用. 北京: 清华大学出版社, 2013) [5] Dai Y Y. Study on the New Cleaner Process of Comprehensive Re鄄 covery of Valuble Metals from Tungsten Residues [ Dissertation]. Changsha: Central South University, 2013 (戴艳阳. 钨渣中有价金属综合回收新清洁工艺研究[学位论 文]. 长沙: 中南大学, 2013) [6] Wang X H, Xiang S B, Zheng S L, et al. A method for extracting potassium tantalum, niobium and potassium fluosilicate from tung鄄 sten smelting slag: China Patent, CN201110240762. 5. 2013鄄鄄 03鄄鄄 06 (王晓辉, 向仕彪, 郑诗礼, 等. 一种从钨冶炼渣中提取钽、铌 并联产氟硅酸钾的方法: 中国专利, CN201110240762. 5. 2013鄄鄄03鄄鄄06) [7] Luo X P, Liu B L, Tang M K. Experimental investigation of com鄄 plex recovery of valuable minerals components containing in the residue abandoned in wet鄄metallurgical process of wolframite ores. China Tungsten Ind, 2005, 20(3): 24 (罗仙平, 刘北林, 唐敏康. 从钨冶炼渣中综合回收有价金属 的试验研究. 中国钨业, 2005, 20(3): 24) [8] Liang W D. Application of two stage autoclave process for higher tungsten metallurgical recovery / / 9th National Hard Alloy Aca鄄 demic Conference. Chengdu, 2006: 117 (梁卫东. 二次压煮工艺提高钨冶炼金属回收率的应用 / / 第 九次全国硬质合金学术会议. 成都, 2006: 117) [9] Du Y. Research on Recovery of Tungsten from Enriched Tungsten Residue [ Dissertation]. Xi蒺an: Xi蒺an University of Architecture and Technology, 2014 (杜阳. 富钨渣中回收钨的研究[学位论文]. 西安: 西安建筑 科技大学, 2014) [10] Wu Y Q, Wu X, Ma G. Tungsten recovery from the residue after acid leaching of superalloy. Min Metall Eng, 2014, 34(6): 101 (吴永谦, 吴贤, 马光. 从某高温合金酸浸渣中回收钨的研 究. 矿冶工程, 2014, 34(6): 101) [11] Yang S H, Wang J, Xie B R, et al. Treatment process of low鄄 grade tungsten slag. Nonferrous Met Sci Eng, 2015, 6(6): 29 (杨少华, 王君, 谢宝如, 等. 低品位钨渣处理工艺. 有色金 属科学与工程, 2015, 6(6): 29) [12] Chen H Z. Recovering tungsten鄄fermanganum from tungsten slag. China Mater Recycl, 1992(8): 42 (陈洪泽. 从钨渣中回收钨钪铁锰. 中国物资再生, 1992 (8): 42) [13] Dai Y Y, Zhong H Y, Li J, et al. Valuable metals蒺 recovery from tungsten residue. J Cent South Univ Technology Nat Sci, 2003, 34(1): 36 (戴艳阳, 钟海云, 李荐, 等. 钨渣中有价金属综合回收工 艺. 中南工业大学学报(自然科学版), 2003, 34(1): 36) [14] Wang J J, Wang X H, Zhang Y, et al. Comprehensive recovery of tantalum and niobium from tantalum鄄niobium residue. Chin J Rare Met, 2015, 39(3): 251 (汪加军, 王晓辉, 张盈, 等. 含钽铌废渣中钽铌资源的综合 回收工艺研究. 稀有金属, 2015, 39(3): 251) [15] Yang X L, Wang X H, Xiang S B, et al. Enrichment of tantalum and niobium from tungsten residue by hydrochloric acid method鄄 he. Chin J Nonferrous Met, 2013, 23(3): 873 (杨秀丽, 王晓辉, 向仕彪, 等. 盐酸法富集钨渣中的钽和 铌. 中国有色金属学报, 2013, 23(3): 873) [16] Xiang S B, Huang B, Wang X H, et al. Research on recovery of tantalum and niobium from tungsten residue by acid method. Nonferrous Met Eng Res, 2012, 33(2): 5 (向仕彪, 黄波, 王晓辉, 等. 从废钨渣中酸法回收钽铌的研 究. 有色冶金设计与研究, 2012, 33(2): 5) [17] Wu B, Shang H, Wen J K. Leaching of niobium from low鄄grade refractory tantalum鄄niobium bearing minerals. Chin J Rare Met, 2013, 37(5): 791 (武彪, 尚鹤, 温建康. 低品位难处理钽铌矿中铌的浸出试 验研究. 稀有金属, 2013, 37(5): 791) [18] Nete M, Purcell W, Nel J T. Non鄄fluoride dissolution of tanta鄄 lum and niobium oxides and their separation using ion exchange. Hydrometallurgy, 2017, 173: 192 [19] Deblonde G J P, Weigel V, Bellier Q, et al. Selective recovery of niobium and tantalum from low鄄grade concentrates using a sim鄄 ple and fluoride鄄free process. Sep Purif Technol, 2016, 162: 180 [20] Kabangu M J, Crouse P L. Separation of niobium and tantalum from Mozambican tantalite by ammonium bifluoride digestion and octanol solvent extraction. Hydrometallurgy, 2012, 129鄄130: 151 [21] Wang W W, Pranolo Y, Cheng C Y. Recovery of scandium from synthetic red mud leach solutions by solvent extraction with D2EHPA. Sep Purif Technol, 2013, 108: 96 [22] Ding C,Wang X H, He C R, et al. Sulfuric acid leaching of scandium from black tungsten ore slag and depression leaching of iron by carphosiderite method. Chin J Process Eng, 2014, 14 (6): 907 (丁冲, 王晓辉, 何超然, 等. 黑钨渣硫酸浸钪及浸出过程中 草黄铁矾法抑制铁浸出. 过程工程学报, 2014, 14(6): 907) [23] Liang H L, Luo D M, Liu C, et al. Leaching of scandium oxide from tungsten slag. Hydrometall China, 2015, 34(2): 114 (梁焕龙, 罗东明, 刘晨, 等. 从钨渣中浸出氧化钪的试验研 究. 湿法冶金, 2015, 34(2): 114) [24] Wang W W, Pranolo Y, Cheng C Y. Metallurgical processes for scandium recovery from various resources: a review. Hydrometal鄄 lurgy, 2011, 108(1鄄2): 100 [25] Vanderpool C D, Huang Y X. Recovery of tungsten ferroscandi鄄 um and manganese from tungsten containing materials. Conserv Utiliz Miner Resour, 1989(1): 42 (Clarence D Vanderpool, 黄永校. 从含钨物料中回收钨钪铁 ·1474·
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