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。590 北京科技大学学报 第31卷 基体内部扩展.在两类裂纹交汇、撕裂过程中,裂纹 系合金组织和性能的影响.金属热处理,2005,47(7):9) 尖端局部区域会发生一定的塑性变形,以协调裂纹 [6 Bae D H.Kim S H.Kim D H,et al.Deformation behavior of Mg-Zn-Y alloys reinfored by icosahedral quasicrystalline parti- 扩展方向,因此在断口表面出现撕裂棱. ds.Ac1Ma1e,2002.50:2343 [7 Bae D H.Lee M H.Kim K T,ct al.Applicat ion of quasicrystah 主裂纹 基体裂纹 ine particles as a strengthening phase in Mg-Zm Y alloys.J Alloys mpd.2002.342:445 [8 Kai YZ.Jie D.Wen JD.et al.Effect of RE content on the frac- 基体裂纹上撕裂分开 ture behavior in Mg-GdNdZr alloys.Mater Sci Forum,2007. 202(1):546 主裂纹 I9 Wu A R.Xia C Q.Gu Y,et al.Research of Mg RE alloy on mi- 图9。裂纹通过撕裂形成台阶的示意图 crostructure and properties.Heat Treat Met,2005.30(8):21 Fig.9 Schematic of forming a sidestep of cracks by tearing (吴安如,夏长清,古一,等.镁-稀土合金的显微组织和力学性 能研究.金属热处理,2005,30(8):21) 10 LiuG Q.Chen L P.Ai Y L,et al.Infhence of Nd on mi- 4结论 crost ructu re and properties of ZM 5 alloys.Spec Cast Non ferrous (1)通过动态拉伸原位观察实验可知,当外加 41l@3,2005,25(7):496 (刘刚强,陈乐平,艾云龙,等.稀土Nd对ZM5合金组织与性 载荷超过1.176kN时,ZK60合金板缺口前端裂纹 能影响的研究.特种铸造及有色合金,2005,25(7):496) 萌生,而ZK60(0.9Y)合金板材加载至1.273kN时 [11]Song M J.W ang Z X.Wang L Y.et al.Superplasticity and 缺口部位萌生裂纹. fractu re mechanism of A231B magnesium alloy sheet.Light A (2)ZK60和ZK60(0.9Y)合金板材宏观断口 loy Fabr Technol,2005,33(8):39 均有解理、准解理断裂痕迹,断口表面都出现小台阶 (宋美娟,王智样,汪凌云,等.AZ31B镁合金板材超塑性变形 与断裂机理研究.轻合金加工技术,2005,33(8):39) 与撕裂岭:随着载荷增大,主裂纹与基体裂纹撕裂贯 [12]Ohr S M.An ekctron micmoscope study of crack tip deformation 通.ZK60合金中主裂纹扩展过程中出现分枝, and its impact on the disbeation theory of fracture.Mater Sci ZK60(0.9Y)合金主裂纹沿第2相扩展,未出现分 Eng,1985,72():1 枝,断口处出现褶皱,基体裂纹多萌生于破碎的第2 [13 Wang X S.Liang F,Zeng Y P,et al.SEM in situ observations 相附近. to the effects of inlusions on initiation and propagation of the low cyclic fatigue crack in super strength steel.Acta Metall Sim,2005,41(12):1272 参考文献 (王习术,梁锋,曾燕屏,等.夹杂物对超高强度钢低周疲劳裂 [1]Decker R F.The menaissance in magnesium.Adv Mater Proass- 纹萌生及扩展影响的原位观测.金属学报,2005,41(12): ,1998.157(9):31 1272) [2]Froes F H,Aghion E,Elezer D,et al.The science technology and [14 Liang C L,Li X Y.Gong S L.et al.Im situ SEM observation applications of magnesium.Ady Perform Mater,1998,5(3): on fracture behavior of laser welded BT20 titanium alloy pints. 201 Rare Met Mater Eng,2006.35(12):1924 [3]Chen Z H.Wrought Magnesium Alloys.Beijing:Chemical In- (粱春雷,李晓延,巩水利,等.SEM原位观察BT20钛合金激 dustry Press 2005 光焊接头的膨裂行为.稀有金属材料与工程,2006,35(12): (陈振华.变形镁合金.北京:化学工业出版社,2005) 1924) [4]Yu K.Li W X,Wang R C.et aL.Research,development and [15]Lu Y Z.Wang Q D.Ding W J.et al.Fracture behavior of application of wrought magnesium alloys.Chin J Nonferrous AZ91 magnesium alloy.Mater Lett,2000,44(5):265 Me,2003,13(2):277 16 Ha K F.Microsopic Theory of Metal Mechanical Properties. (余琨,黎文献,王日初,等.变形镁合金的研究、开发及应用.中 Beijing Science Press,1983 国有色金属学报,2003.13(2):277) (哈宽富.金属力学性质的微观理论.北京:科学出版社, [5]Wang B.Yi D Q.Fang X Y.et al.Influence of Y and Nd on 1983) Miemstnucture and Pmoperies of Mg-Zn-Zr Alloys Heat Treat I 17]Bae D H.Kim D H,Kim W T,et al.High strength Mg-Zn-Y Me,2005,47(7):9 alloy contairing quasicrystalline particles.Mater Trans,2001. (王斌,易丹青,方西亚,等.稀土元素Y和Nd对Mg一Z一Zr 42(10):2144基体内部扩展.在两类裂纹交汇 、撕裂过程中, 裂纹 尖端局部区域会发生一定的塑性变形, 以协调裂纹 扩展方向, 因此在断口表面出现撕裂棱 . 图 9 裂纹通过撕裂形成台阶的示意图 Fig.9 S chematic of forming a sidestep of cracks by tearing 4 结论 (1) 通过动态拉伸原位观察实验可知, 当外加 载荷超过 1.176 kN 时, ZK60 合金板缺口前端裂纹 萌生, 而ZK60( 0.9Y) 合金板材加载至 1.273 kN 时 缺口部位萌生裂纹. ( 2) ZK60 和 ZK60( 0.9Y) 合金板材宏观断口 均有解理 、准解理断裂痕迹, 断口表面都出现小台阶 与撕裂岭 ;随着载荷增大, 主裂纹与基体裂纹撕裂贯 通.ZK60 合金中主裂纹扩展过程中出现分枝, ZK60( 0.9Y) 合金主裂纹沿第 2 相扩展, 未出现分 枝, 断口处出现褶皱, 基体裂纹多萌生于破碎的第 2 相附近. 参 考 文 献 [ 1] Decker R F .The renaissance in magnesium .Adv Mater Process￾es, 1998, 157( 9) :31 [ 2] Froes F H,Aghion E, Eliezer D, et al.The science technology and applications of magnesium .Adv Perform Mater, 1998, 5 ( 3) : 201 [ 3] Chen Z H .Wrought Magnesium Alloys.Beijing :Chemical In￾dustry Press, 2005 ( 陈振华.变形镁合金.北京:化学工业出版社, 2005) [ 4] Yu K, Li W X, Wang R C, et al.Research, development and application of w rough t magnesium alloys.Chin J Non f errous Met, 2003, 13( 2) :277 ( 余琨, 黎文献, 王日初, 等.变形镁合金的研究、开发及应用.中 国有色金属学报, 2003, 13( 2) :277) [ 5] Wang B, Yi D Q, Fang X Y, et al.Influence of Y and Nd on Microstructure and Properties of Mg-Zn-Zr Alloys.Heat Treat Met, 2005, 47( 7) :9 ( 王斌, 易丹青, 方西亚, 等.稀土元素 Y 和 Nd 对 Mg -Zn-Zr 系合金组织和性能的影响.金属热处理, 2005, 47( 7) :9) [ 6] Bae D H, Kim S H, Kim D H, et al.Deformati on behavior of Mg-Zn-Y alloys reinf orced by icosahedral quasicrystalline parti￾cles.Acta Mater, 2002, 50:2343 [ 7] Bae D H, Lee M H, Kim K T, et al.Application of quasicrystal￾line particles as a strengthening phase in Mg-Zn-Y alloys.J Alloys Compd , 2002, 342:445 [ 8] Kai Y Z, Jie D,Wen J D, et al.Effect of RE cont ent on the frac￾ture behavior in Mg-Gd-Nd-Zr alloys.Mater S ci For um , 2007, 202( 1) :546 [ 9] Wu A R, Xia C Q, Gu Y, et al.Research of Mg-RE alloy on mi￾crostructu re and properties.Heat Treat Met, 2005, 30( 8) :21 ( 吴安如, 夏长清,古一, 等.镁-稀土合金的显微组织和力学性 能研究.金属热处理, 2005, 30( 8) :21) [ 10] LiuG Q, Chen L P, Ai Y L, et al.Influence of Nd on mi￾crostructu re and properties of ZM 5 alloys.S pec Cast Non ferrous Alloys, 2005, 25( 7) :496 ( 刘刚强, 陈乐平, 艾云龙, 等.稀土 Nd对 ZM5 合金组织与性 能影响的研究.特种铸造及有色合金, 2005, 25( 7) :496) [ 11] Song M J, Wang Z X, Wang L Y, et al.Superplasticity and fractu re mechanism of AZ31B magnesium alloy sheet .Light A l￾loy Fabr Technol, 2005, 33( 8) :39 ( 宋美娟, 王智祥, 汪凌云, 等.AZ31B 镁合金板材超塑性变形 与断裂机理研究.轻合金加工技术, 2005, 33( 8) :39) [ 12] Oh r S M .An electron microscope study of crack tip def ormation and its impact on the dislocation theory of fracture.Mater Sci Eng , 1985, 72( 1) :1 [ 13] Wang X S, Liang F, Zeng Y P, et al.SEM in situ observations to the effects of inclusions on initiation and propagation of the low cyclic f atigue crack in super strength steel.Acta Metall S in , 2005, 41( 12) :1272 ( 王习术, 梁锋, 曾燕屏, 等.夹杂物对超高强度钢低周疲劳裂 纹萌生及扩展影响的原位观测.金属学报, 2005, 41 ( 12 ) : 1272) [ 14] Liang C L, Li X Y, Gong S L, et al.In-situ SEM observation on fracture behavior of laser w elded BT20 tit anium alloy joints. Rare Met Mater Eng , 2006, 35( 12) :1924 ( 梁春雷, 李晓延, 巩水利, 等.SEM 原位观察 BT20 钛合金激 光焊接头的断裂行为.稀有金属材料与工程, 2006, 35( 12 ) : 1924) [ 15] Lu Y Z, Wang Q D, Ding W J, et al.Fracture behavior of AZ91 magnesium alloy .Mater Lett, 2000, 44( 5) :265 [ 16] Ha K F .Microscopic Theory o f Metal Mechani cal Properties . Beijing:Science Press, 1983 ( 哈宽富.金属力学性质的微观理论.北京:科学出版社, 1983) [ 17] Bae D H, Kim D H, Kim W T, et al.High strength Mg-Zn-Y alloy containing quasicrystalline particles.Mater Trans, 2001, 42( 10) :2144 · 590 · 北 京 科 技 大 学 学 报 第 31 卷
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