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.738. 北京科技大学学报 第31卷 数kp为1.1275×10-12g2cm4min1. [7]Zhang X F.Lu A X.Zhang H X.Research on the bonding mech- (3)粒径为40m、镀铜增重10%的金刚石颗 anism at interface between vitrified bond and diamond.Diamond 粒在上述气氛中氧化时，氧化时间应小于358min, Abrasives Eng.2007.159(3):43 (张小福，卢安贤，张红霞·陶瓷结合剂与金刚石高温下的界面 本实验选取氧化时间为40min,可在金刚石表面获 结合机理研究.金刚石与磨料磨具工程，2007,159(3)：43) 得CuCu20的复合结构. [8]Zhang X F.Lu A X.Zhang H X.Research on soakage between ceramic glass bond and diamond at high temperature.Diamond 参考文献 Abrasives Eng.2007.157(1):44 (张小福，卢安贤，张红霞.高温下微晶玻璃结合剂对金刚石磨 [1]Yoshida K.Morigami H.Thermal properties of diamond/copper 料润湿性研究·金刚石与磨料磨具工程，2007,157(1)：44) composite material.Microelectron Reliab,2004.44(2):303 [9]Shilo A E,Bondarev E K.Composite diamond-containing tool [2]Ekimov E A.Suetin N V,Popovich A F.et al.Thermal condue- materials in a glassy binder.ISuperhard Mater,2000.22(5): tivity of diamond composites sintered under high pressures.Dia 19 mond Relat Mater,2008.17(5):838 [10]Williams C T,Demetry C.Li R.Structure and strength of in- [3]Schubert T.Ciupinski L.Zielinski W.et al.Interfacial charac- terfaces in titanium-coated diamond-glass composites.Ceram terization of Cu/diamond composites prepared by powder metal- Eng Sei Proc,2000,21(3):697 lurgy for heat sink application.Scripta Mater.2008.58(4): [11]Toshikazu A,Tomoko A.Glass sealing technology by using 263 Dumet.Matsushita Tech J.2001,47(4):63 [4]Shimono M.Kume S.HIP-sintered composites of C(diamond)/ [12]Liang Y J.Physical Chemistry.Beijing:Metallurgical Industry SiC.J Am Ceram Soc,2004,87(4):752 Press,1989 [5]Mlungwane K.Herrmann M,Sigalas I.The low pressure infil- (梁英教.物理化学.北京：冶金工业出版社，1989) tration of diamond by silicon to form diamond-silicon carbide com- [13]Zhu RZ.He Y D,Qi H B.High Temperature Corrosion and posites.J Eur Ceram Soc,2008.28(1):321 High Temperature Corrosion Resistant Materials.Shanghai: [6]Lin K H.PengS F.Lin$T.Sintering parameters and wear per- Shanghai Science and Technology Press.1995 formances of vitrified bond diamond grinding wheels.Int Re- (朱日彰，何业东，齐慧滨。高温腐蚀及耐高温腐蚀材料。上 fract Met Hard Mater,2007.25(1):25 海：上海科学技术出版社，1995)数 kp 为1∙1275×10－12 g 2·cm －4·min －1． （3） 粒径为40μm、镀铜增重10％的金刚石颗 粒在上述气氛中氧化时氧化时间应小于358min． 本实验选取氧化时间为40min可在金刚石表面获 得 Cu－Cu2O 的复合结构． 参 考 文 献 ［1］ Yoshida KMorigami H．Thermal properties of diamond／copper composite material．Microelectron Reliab200444（2）：303 ［2］ Ekimov E ASuetin N VPopovich A Fet al．Thermal conductivity of diamond composites sintered under high pressures．Diamond Relat Mater200817（5）：838 ［3］ Schubert TCiupiński LZieliński Wet al．Interfacial characterization of Cu／diamond composites prepared by powder metallurgy for heat sink application．Scripta Mater200858（4）： 263 ［4］ Shimono MKume S．HIP-sintered composites of C （diamond）／ SiC．J A m Ceram Soc200487（4）：752 ［5］ Mlungwane KHerrmann MSigalas I．The low-pressure infiltration of diamond by silicon to form diamond-silicon carbide composites．J Eur Ceram Soc200828（1）：321 ［6］ Lin K HPeng S FLin S T．Sintering parameters and wear performances of vitrified bond diamond grinding wheels．Int J Ref ract Met Hard Mater200725（1）：25 ［7］ Zhang X FLu A XZhang H X．Research on the bonding mechanism at interface between vitrified bond and diamond．Diamond Abrasives Eng2007159（3）：43 （张小福卢安贤张红霞．陶瓷结合剂与金刚石高温下的界面 结合机理研究．金刚石与磨料磨具工程2007159（3）：43） ［8］ Zhang X FLu A XZhang H X．Research on soakage between ceramic glass bond and diamond at high temperature．Diamond Abrasives Eng2007157（1）：44 （张小福卢安贤张红霞．高温下微晶玻璃结合剂对金刚石磨 料润湿性研究．金刚石与磨料磨具工程2007157（1）：44） ［9］ Shilo A EBondarev E K．Composite diamond-containing tool materials in a glassy binder．J Superhard Mater200022（5）： 19 ［10］ Williams C TDemetry CLi R．Structure and strength of interfaces in titanium-coated diamond-glass composites． Ceram Eng Sci Proc200021（3）：697 ［11］ Toshikazu ATomoko A．Glass sealing technology by using Dumet．Matsushita Tech J200147（4）：63 ［12］ Liang Y J．Physical Chemistry．Beijing：Metallurgical Industry Press1989 （梁英教．物理化学．北京：冶金工业出版社1989） ［13］ Zhu R ZHe Y DQi H B．High Temperature Corrosion and High Temperature Corrosion Resistant Materials．Shanghai： Shanghai Science and Technology Press1995 （朱日彰何业东齐慧滨．高温腐蚀及耐高温腐蚀材料．上 海：上海科学技术出版社1995） ·738· 北 京 科 技 大 学 学 报 第31卷