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第36卷第4期 北京科技大学学报 Vol.36 No.4 2014年4月 Journal of University of Science and Technology Beijing Apr.2014 伪半固态触变成形制备SiCp/Al电子封装材料的组织 与性能 郭明海,刘俊友”,贾成厂”,果世驹”,李艳霞》,周洪宇 1)北京科技大学材料科学与工程学院,北京1000832)北华航天工业学院材料系,廊坊065000 ☒通信作者,E-mail:qifeng_guo(@126.com 摘要采用伪半固态触变成形工艺制备了40%、56%和63%三种不同SiC体积分数颗粒增强A1基电子封装材料,并借助 光学显微镜和扫描电镜分析了材料中A!和Si汇的形态分布及其断口形貌,测定了材料的密度、致密度、热导率、热膨胀系数、 抗压强度和抗弯强度.结果表明,通过伪半固态触变成形工艺可制备出的不同SC体积分数A!基电子封装材料,其致密度 高,热膨胀系数可控,材料中A1基体相互连接构成网状,SC颗粒均匀镶嵌分布于A1基体中.随着SC颗粒体积分数的增加, 电子封装材料密度和室温下的热导率稍有增加,热膨胀系数逐渐减小,室温下的抗压强度和抗弯强度逐渐增加.SC/A1电子 封装材料的断裂方式为SiC的脆性断裂,同时伴随着A!基体的韧性断裂. 关键词电子封装;颗粒增强复合材料:触变成形;热导率;热膨胀:材料强度 分类号TN405 Microstructure and properties of SiCp/Al electronic packaging materials fabricated by pseudo-semi-solid thixoforming GUO Ming-hai,LIU Jun-you,JIA Cheng-chang",GUO Shi-ju,LI Yan-xia,ZHOU Hong-yu) 1)School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing 100083,China 2)Department of Materials,North China Institute of Aerospace Engineering,Langfang 065000,China Corresponding author,E-mail:qifeng_guo@126.com ABSTRACT SiC particles reinforced Al matrix composites with three different SiC volume fractions of 40%,56%and 63%for elec- tronic packaging were prepared by pseudo-semi-solid thixoforming.The Al and SiC distribution and the fractographs of the SiCp/Al electronic packaging materials were examined by optical microscopy and scanning electron microscopy.The density,relative density, thermal conductivity (TC),coefficient of thermal expansion (CTE),compressive strength and bending strength of the SiCp/Al elec- tronic packaging materials were tested.It is found that the SiCp/Al electronic packaging materials have controllable coefficients of ther- mal expansion and high relative density.The Al matrix is connected into a network,and SiC particles are uniformly distributed in the Al matrix.When the SiC volume fraction increases,the density and thermal conductivity at room temperature lightly increase,the coef- ficient of thermal expansion gradually decreases,and the compressive strength and bending strength increase.The main fracture mode of the SiC/Al electronic packaging materials is brittle fracture of SiC particles accompanied by ductile fracture of the Al matrix at the same time. KEY WORDS electronic packaging:particle reinforced composites:thixoforming:thermal conductivity:thermal expansion:strength of materials 半导体集成电路的速度和集成度提高,导致芯元件的失效率与其工作温度呈指数关系,功能则与 片发热率增加,电路工作温度上升.实验证明,单个 其成反比口,因而如何提高芯片的散热效率,使得 收稿日期:201304-一17 DOI:10.13374/j.issn1001-053x.2014.04.011:http:/jourals.ustb.edu.cn第 36 卷 第 4 期 2014 年 4 月 北京科技大学学报 Journal of University of Science and Technology Beijing Vol. 36 No. 4 Apr. 2014 伪半固态触变成形制备 SiCp /Al 电子封装材料的组织 与性能 郭明海1) ,刘俊友1) ,贾成厂1) ,果世驹1) ,李艳霞2) ,周洪宇1) 1) 北京科技大学材料科学与工程学院,北京 100083 2) 北华航天工业学院材料系,廊坊 065000  通信作者,E-mail: qifeng_guo@ 126. com 摘 要 采用伪半固态触变成形工艺制备了 40% 、56% 和 63% 三种不同 SiC 体积分数颗粒增强 Al 基电子封装材料,并借助 光学显微镜和扫描电镜分析了材料中 Al 和 SiC 的形态分布及其断口形貌,测定了材料的密度、致密度、热导率、热膨胀系数、 抗压强度和抗弯强度. 结果表明,通过伪半固态触变成形工艺可制备出的不同 SiC 体积分数 Al 基电子封装材料,其致密度 高,热膨胀系数可控,材料中 Al 基体相互连接构成网状,SiC 颗粒均匀镶嵌分布于 Al 基体中. 随着 SiC 颗粒体积分数的增加, 电子封装材料密度和室温下的热导率稍有增加,热膨胀系数逐渐减小,室温下的抗压强度和抗弯强度逐渐增加. SiC/Al 电子 封装材料的断裂方式为 SiC 的脆性断裂,同时伴随着 Al 基体的韧性断裂. 关键词 电子封装; 颗粒增强复合材料; 触变成形; 热导率; 热膨胀; 材料强度 分类号 TN405 Microstructure and properties of SiCp /Al electronic packaging materials fabricated by pseudo-semi-solid thixoforming GUO Ming-hai 1)  ,LIU Jun-you1) ,JIA Cheng-chang1) ,GUO Shi-ju1) ,LI Yan-xia2) ,ZHOU Hong-yu1) 1) School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing 100083,China 2) Department of Materials,North China Institute of Aerospace Engineering,Langfang 065000,China  Corresponding author,E-mail: qifeng_guo@ 126. com ABSTRACT SiC particles reinforced Al matrix composites with three different SiC volume fractions of 40% ,56% and 63% for elec￾tronic packaging were prepared by pseudo-semi-solid thixoforming. The Al and SiC distribution and the fractographs of the SiCp /Al electronic packaging materials were examined by optical microscopy and scanning electron microscopy. The density,relative density, thermal conductivity ( TC) ,coefficient of thermal expansion ( CTE) ,compressive strength and bending strength of the SiCp /Al elec￾tronic packaging materials were tested. It is found that the SiCp /Al electronic packaging materials have controllable coefficients of ther￾mal expansion and high relative density. The Al matrix is connected into a network,and SiC particles are uniformly distributed in the Al matrix. When the SiC volume fraction increases,the density and thermal conductivity at room temperature lightly increase,the coef￾ficient of thermal expansion gradually decreases,and the compressive strength and bending strength increase. The main fracture mode of the SiC/Al electronic packaging materials is brittle fracture of SiC particles accompanied by ductile fracture of the Al matrix at the same time. KEY WORDS electronic packaging; particle reinforced composites; thixoforming; thermal conductivity; thermal expansion; strength of materials 收稿日期: 2013--04--17 DOI: 10. 13374 /j. issn1001--053x. 2014. 04. 011; http: / /journals. ustb. edu. cn 半导体集成电路的速度和集成度提高,导致芯 片发热率增加,电路工作温度上升. 实验证明,单个 元件的失效率与其工作温度呈指数关系,功能则与 其成反比[1],因而如何提高芯片的散热效率,使得
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