·1614 工程科学学报,第39卷,第11期 [11]Fang JJ,Yang N,Cen D Y,et al.Odor compounds from differ- mospheric volatile organic pollutants by thermal desorption gas ent sources of landfill:characterization and source identification. chromatography mass spectrometry.Anal Methods,2013.5:219 Waste Manage,2012,32(7):1401 7]Kim Y H,Kim K H.An accurate and reliable analysis of trime- [12]Romain A C,Delva J,Nicolas J.Complementary approaches to thylamine using thermal desorption and gas chromatography-ime measure environmental odours emitted by landfill areas.Sens Ac- of flight mass spectrometry.Anal Chim Acta,2013,780:46 ators B:Chem,2008,131(1):18 [28]Ras M R,Borrull F,Marce R M.Determination of volatile or- [13]Lakhouit A,Schirmer W N.Johnson T R,et al.Evaluation of ganic sulfur compounds in the air at sewage management areas by the efficiency of an experimental biocover to reduce BTEX emis- thermal desorption and gas chromatography-mass spectrometry. sions from landfill biogas.Chemosphere,2014,97:98 Talanta,2008,74(4):562 [14]Capanema M A,Cabana H,Cabral A R.Reduction of odours in 29]Mochalski P,Wzorek B,Sliwka I,et al.Improved pre-concen- pilot-scale landfill biocovers.Waste Manage,2014,34(4):770 tration and detection methods for volatile sulphur breath constitu- [15]Xu Q Y,Powell J,Jain P,et al.Modeling of H2S migration ents.J Chromatogr B,2009,877(20-21):1856 through landfill cover materials.J Hazard Mater,2014,264: B0]Lestremau F,Andersson F A T,Desauziers V.Investigation of 254 artefact formation during analysis of volatile sulphur compounds [16]Gallego E,Perales J F,Roca F J,et al.Surface emission deter- using solid phase microextraction (SPME).Chromatographia, mination of volatile organic compounds (VOC)from a closed in- 2004,59(910):607 dustrial waste landfill using a self-designed static flux chamber. B1]Andersen K B,Hansen M J,Feilberg A.Minimisation of artefact Sci Total Enriron,2014,470-471:587 formation of dimethyl disulphide during sampling and analysis of [17]Marti V,Jubany I.Perez C,et al.Human health risk assess- methanethiol in air using solid sorbent materials.J Chromatogr ment of a landfill based on volatile organic compounds emission, A,2012,1245:24 immission and soil gas concentration measurements.Appl Geo- B2]Musteata F M,Pawliszyn J.Bioanalytical applications of solid- chem,2014,49:218 phase microextraction.TrAC,Trends Anal Chem,2007,26(1): [18]Parker D.Ham J,Woodbury B,et al.Standardization of flux 36 chamber and wind tunnel flux measurements for quantifying vola- B3]Pacolay B D,Ham J E,Wells J R.Use of solid-phase microex- tile organic compound and ammonia emissions from area sources traction to detect and quantify gas-phase dicarbonyls in indoor en- at animal feeding operations.Atmos Enriron,2013,66:72 vironments.J Chromatogr A,2006,1131 (12):275 [19]Liu Y J,Lu W J,Li D,et al.Estimation of volatile compounds 34]Domeno C,Martinez-Garcia F,Campo L,et al.Sampling and a- emission rates from the working face of a large anaerobic landfill nalysis of volatile organic pollutants emitted by an industrial in China using a wind tunnel system.Atmos Entiron,2015, stack.Anal Chim Acta,2004,524(12):51 111:213 B5]Kabir E,Kim K H.Use of solid phase microextraction (SPME) [20]Parker D B,Caraway E A,Rhoades M B,et al.Effect of wind in the analysis of the reduced sulfur compounds (RSC)and its tunnel air velocity on VOC flux from standard solutions and experimental limitations.Microchem J,2012,103:42 CAFO manure/wastewater.Trans Asabe,2010,53 (3):831 B6] Iwasaki Y.The history of odor measurement in Japan and triangle 1]Wang B,Sivret EC.Paresi G,et al.Reduced sulfur compounds odor bag method.Odor Meas Rev,2003:37 in the atmosphere of sewer networks in Australia:geographic B7] Nagata Y.Measurement of odor threshold by triangle odor bag (and seasonal)variations.Water Sci Technol,2014,69(6): method.Odor Meas Rer,2003:118 1167 B8] Hansen M J,Jonassen K E N,Lakke MM,et al.Multivariate 22]Brown V M,Crump D R,Plant N T,et al.Evaluation of the prediction of odor from pig production based on in-situ measure- stability of a mixture of volatile organic compounds on sorbents for ment of odorants.Atmos Enriron,2016,135:50 the determination of emissions from indoor materials and products B9] Blazy V,de Guardia A,Benoist J C,et al.Odorous gaseous e- using thermal desorption/gas chromatography/mass spectrometry missions as influence by process condition for the forced aeration JChromatogr A,2014,1350:1 composting of pig slaughterhouse sludge.Waste Manage,2014, 23]Szulejko JE,Kim K H.A review of sampling and pretreatment 34(7):1125 techniques for the collection of airbomne amines.TrAC,Trends [40]Kim Y H,Kim K H,Szulejko J E,et al.Quantitative analysis of Anal Chem,2014,57:118 fragrance and odorants released from fresh and decaying strawber- 4]Brown A S,van der Veen A M H,Arhenius K,et al.Sampling ies.Sens,2013,13(6):7939 of gaseous sulfur-containing compounds at low concentrations with [41]Jo S H,Kim K H,Jeon B H,et al.Odor characterization from a review of best-practice methods for biogas and natural gas appli- bams and slurry treatment facilities at a commercial swine facility cations.TrAC Trends Anal Chem,2015,64:42 in South Korea.Atmos Enriron,2015,119:339 5]Woolfenden E.Sorbent-ased sampling methods for volatile and [42] Scaglia B,Orzi V,Artola A,et al.Odours and volatile organic semi-volatile organie compounds in air.Part 2.Sorbent selection compounds emitted from municipal solid waste at different stage and other aspects of optimizing air monitoring methods.J Chrom- of decomposition and relationship with biological stability.Biore- atogr A,2010,1217(16):2685 sour Technol,2011,102(7):4638 26]Wong G K S,Ng S J,Webster R D.Quantitative analysis of at- [43] Akdeniz N,Jacobson L D,Hetchler B P,et al.Odor and odor-工程科学学报,第 39 卷,第 11 期 [11] Fang J J,Yang N,Cen D Y,et al. Odor compounds from different sources of landfill: characterization and source identification. Waste Manage,2012,32( 7) : 1401 [12] Romain A C,Delva J,Nicolas J. Complementary approaches to measure environmental odours emitted by landfill areas. Sens Actuators B: Chem,2008,131( 1) : 18 [13] Lakhouit A,Schirmer W N,Johnson T R,et al. Evaluation of the efficiency of an experimental biocover to reduce BTEX emissions from landfill biogas. Chemosphere,2014,97: 98 [14] Capanema M A,Cabana H,Cabral A R. Reduction of odours in pilot-scale landfill biocovers. Waste Manage,2014,34( 4) : 770 [15] Xu Q Y,Powell J,Jain P,et al. Modeling of H2 S migration through landfill cover materials. J Hazard Mater,2014,264: 254 [16] Gallego E,Perales J F,Roca F J,et al. Surface emission determination of volatile organic compounds ( VOC) from a closed industrial waste landfill using a self-designed static flux chamber. Sci Total Environ,2014,470-471: 587 [17] Martí V,Jubany I,Pérez C,et al. Human health risk assessment of a landfill based on volatile organic compounds emission, immission and soil gas concentration measurements. Appl Geochem,2014,49: 218 [18] Parker D,Ham J,Woodbury B,et al. Standardization of flux chamber and wind tunnel flux measurements for quantifying volatile organic compound and ammonia emissions from area sources at animal feeding operations. Atmos Environ,2013,66: 72 [19] Liu Y J,Lu W J,Li D,et al. Estimation of volatile compounds emission rates from the working face of a large anaerobic landfill in China using a wind tunnel system. Atmos Environ,2015, 111: 213 [20] Parker D B,Caraway E A,Rhoades M B,et al. Effect of wind tunnel air velocity on VOC flux from standard solutions and CAFO manure /wastewater. Trans Asabe,2010,53( 3) : 831 [21] Wang B,Sivret E C,Parcsi G,et al. Reduced sulfur compounds in the atmosphere of sewer networks in Australia: geographic ( and seasonal) variations. Water Sci Technol,2014,69 ( 6) : 1167 [22] Brown V M,Crump D R,Plant N T,et al. Evaluation of the stability of a mixture of volatile organic compounds on sorbents for the determination of emissions from indoor materials and products using thermal desorption /gas chromatography /mass spectrometry. J Chromatogr A,2014,1350: 1 [23] Szulejko J E,Kim K H. A review of sampling and pretreatment techniques for the collection of airborne amines. TrAC,Trends Anal Chem,2014,57: 118 [24] Brown A S,van der Veen A M H,Arrhenius K,et al. Sampling of gaseous sulfur-containing compounds at low concentrations with a review of best-practice methods for biogas and natural gas applications. TrAC Trends Anal Chem,2015,64: 42 [25] Woolfenden E. Sorbent-based sampling methods for volatile and semi-volatile organic compounds in air. Part 2. Sorbent selection and other aspects of optimizing air monitoring methods. J Chromatogr A,2010,1217( 16) : 2685 [26] Wong G K S,Ng S J,Webster R D. Quantitative analysis of atmospheric volatile organic pollutants by thermal desorption gas chromatography mass spectrometry. Anal Methods,2013,5: 219 [27] Kim Y H,Kim K H. An accurate and reliable analysis of trimethylamine using thermal desorption and gas chromatography-time of flight mass spectrometry. Anal Chim Acta,2013,780: 46 [28] Ras M R,Borrull F,Marce R M. Determination of volatile organic sulfur compounds in the air at sewage management areas by thermal desorption and gas chromatography-mass spectrometry. Talanta,2008,74( 4) : 562 [29] Mochalski P,Wzorek B,Sliwka I,et al. Improved pre-concentration and detection methods for volatile sulphur breath constituents. J Chromatogr B,2009,877( 20-21) : 1856 [30] Lestremau F,Andersson F A T,Desauziers V. Investigation of artefact formation during analysis of volatile sulphur compounds using solid phase microextraction ( SPME) . Chromatographia, 2004,59( 9-10) : 607 [31] Andersen K B,Hansen M J,Feilberg A. Minimisation of artefact formation of dimethyl disulphide during sampling and analysis of methanethiol in air using solid sorbent materials. J Chromatogr A,2012,1245: 24 [32] Musteata F M,Pawliszyn J. Bioanalytical applications of solidphase microextraction. TrAC,Trends Anal Chem,2007,26( 1) : 36 [33] Pacolay B D,Ham J E,Wells J R. Use of solid-phase microextraction to detect and quantify gas-phase dicarbonyls in indoor environments. J Chromatogr A,2006,1131( 1-2) : 275 [34] Domeno C,Martínez-García F,Campo L,et al. Sampling and analysis of volatile organic pollutants emitted by an industrial stack. Anal Chim Acta,2004,524( 1-2) : 51 [35] Kabir E,Kim K H. Use of solid phase microextraction ( SPME) in the analysis of the reduced sulfur compounds ( RSC) and its experimental limitations. Microchem J,2012,103: 42 [36] Iwasaki Y. The history of odor measurement in Japan and triangle odor bag method. Odor Meas Rev,2003: 37 [37] Nagata Y. Measurement of odor threshold by triangle odor bag method. Odor Meas Rev,2003: 118 [38] Hansen M J,Jonassen K E N,Lkke M M,et al. Multivariate prediction of odor from pig production based on in-situ measurement of odorants. Atmos Environ,2016,135: 50 [39] Blazy V,de Guardia A,Benoist J C,et al. Odorous gaseous emissions as influence by process condition for the forced aeration composting of pig slaughterhouse sludge. Waste Manage,2014, 34( 7) : 1125 [40] Kim Y H,Kim K H,Szulejko J E,et al. Quantitative analysis of fragrance and odorants released from fresh and decaying strawberries. Sens,2013,13( 6) : 7939 [41] Jo S H,Kim K H,Jeon B H,et al. Odor characterization from barns and slurry treatment facilities at a commercial swine facility in South Korea. Atmos Environ,2015,119: 339 [42] Scaglia B,Orzi V,Artola A,et al. Odours and volatile organic compounds emitted from municipal solid waste at different stage of decomposition and relationship with biological stability. Bioresour Technol,2011,102( 7) : 4638 [43] Akdeniz N,Jacobson L D,Hetchler B P,et al. Odor and odor- · 4161 ·