·1144· 工程科学学报，第38卷，第8期 2]Justin P,Meher S K.Rao G R.Tuning of capacitance behavior electrooxidation:mesoporous vs.nanoparticulate.Int Hydrogen of NiO using anionic,cationic,and nonionic surfactants by hy- Energy,2014,39(21):10892 drothermal synthesis.J Phys Chem C,2010,114(11):5203 [17]Shamsipur M,Najafi M,Hosseini M R M.Electrooxidation of al- [13]Needham S A,Wang G X,Liu H K.Synthesis of Ni nanotubes cohols at a nickel oxide/multi-walled carbon nanotube-modified for use as negative electrodes in lithium ion batteries.J Power glassy carbon electrode.J Appl Electrochem,2013,43 (10): Sources,2006,159(1):254 1027 [14]Dirksen JA,Duwal K,Ring T A.NiO thin-film formaldehyde [18]Sing KS W.Reporting physisorption data for gas/solid systems gas sensor.Sens Actuators B,2001,80(2)106 with special reference to the determination of surface area and po- [15]Tong X L,Qin Y,Guo X Y.Enhancedcatalytic activity for rosity.Pure Appl Chem,1985,57(4):603 methanol electro-xidation of uniformly dispersed nickel oxide [19]Yang J H,Tan J,Yang F,et al.Electro-oxidation of methanol nanoparticles -carbon nanotube hybrid materials.Small, on mesoporous nickel phosphate modified GCE.Electrochem 2012,8(2):3390 Commun,2012,23:13 [16]Gu D C,Huang M L,Ge X,et al.NiO electrode for methanol工程科学学报，第 38 卷，第 8 期 ［12］ Justin P，Meher S K，Ｒao G Ｒ． Tuning of capacitance behavior of NiO using anionic，cationic，and nonionic surfactants by hy￾drothermal synthesis． J Phys Chem C，2010，114( 11) : 5203 ［13］ Needham S A，Wang G X，Liu H K． Synthesis of NiO nanotubes for use as negative electrodes in lithium ion batteries． J Power Sources，2006，159( 1) : 254 ［14］ Dirksen J A，Duwal K ，Ｒing T A． NiO thin-film formaldehyde gas sensor． Sens Actuators B，2001，80( 2) : 106 ［15］ Tong X L，Qin Y，Guo X Y． Enhancedcatalytic activity for methanol electro-oxidation of uniformly dispersed nickel oxide nanoparticles — carbon nanotube hybrid materials． Small， 2012，8( 2) : 3390 ［16］ Gu D C，Huang M L，Ge X，et al． NiO electrode for methanol electro-oxidation: mesoporous vs． nanoparticulate． Int J Hydrogen Energy，2014，39( 21) : 10892 ［17］ Shamsipur M，Najafi M，Hosseini M Ｒ M． Electrooxidation of al￾cohols at a nickel oxide /multi-walled carbon nanotube-modified glassy carbon electrode． J Appl Electrochem，2013，43 ( 10 ) : 1027 ［18］ Sing K S W． Ｒeporting physisorption data for gas/ solid systems with special reference to the determination of surface area and po￾rosity． Pure Appl Chem，1985，57( 4) : 603 ［19］ Yang J H，Tan J，Yang F，et al． Electro-oxidation of methanol on mesoporous nickel phosphate modified GCE． Electrochem Commun，2012，23: 13 · 4411 ·