第1期 王嵬,等:地沟油鉴别检测方法研究进展 223 医大学学报,2011,33(13):1366-1369 2009,34(3):75-77 an L, Zhou Y, Zhu JD, et al. Acute toxicity and genetic toxicity of Ji L, Che ZM, Li MY. Rapid distinguishing of swill on by conductivity ogwash fat P). J Third Milit Med Univ, 2011, 33(13): 1366-1369 determination P]. China Oil Fat, 2009, 34(3): 75-77 8]卢海燕,王欣,赵婷婷,等.“地沟油”常见检测方法及低场核磁共振法 9彭进,黄道平,刘吉星,等.电导率的测定在鉴别潲水油中的应用研究 的研究进展印.食品安全质量检测学报,2013,4(5)1428-1436 实用预防医学,2007,14(3:878-879 Lu HY, Wang x, Zhao TT, et al. Research progress on the common Peng J, Huang DP, Liu Jx, et al. Application study of electrica detection methods and LF-NMR of illegal cooked oil pJ J Food Saf Qual conductivity measurement in hogwash oil identification P]. Pr Pre Med 2013,4(5):1428-14 2007,14(3)878-879 9]胡小泓,稍水油鉴别方法的研究食品工业,2010,4:98-100 20]胡小泓,刘志金,郑雪玉,等.应用电导率检测潲水油方法的研究 Hu XH. Study on the Identification method of Slightly water oil P]. Food 食品科学,2007,28(11:482-484 nd,2010,4:98-100. Hu XH, Liu Z, Zhen XY, et al. Research on electroconductivity detection 王乐,刘尧刚,陈凤飞,等,地沟油的污染及变质情况研究武汉工 of hogwash fat P]. Food Sci, 2007, 28(11): 482-484 业学院学报,2007,26(4):1-4. [21]任佳丽,刘振华,李忠海,等.利用压电换能器快速鉴别潲水油食 Wang L, Liu YG, Chen FF, et al. Study on pollution and deterioration of 品与机械,2011,27(2):62-64 the illegal cooked oil P).J Wuhan Polytech Univ, 2007, 26(4): 1-4. Ren JL, Liu ZH, Li Zw, ef al. The rapid identification of swill oil by 「!]曹维金,杨永存,招辉,等,基于常规指标鉴别地沟油”与食用植物油 piezoelectric transducer P]. Food Mach, 2011, 27(2): 62-64. 的有效性评估卫生研究,2014,(43)2:311-312 [2]李红,屠大伟,李根容,等.固相微萃取及主成分分析用于潲水油 Chao WJ, Yang YC, Zhao H, et al. The effectiveness evaluation of based GCMS指纹图谱的分析计量学报,2010,31(5):101-105. on the conventional indexes to identify "illegal cooked oil "and edible Li H, Tu Dw, Li GR, ef al. SPEM and principal component analysis of vegetable oil P). J Hyg Res, 2014, (43)2: 311-312 hogwash oil GC-MS fingerprint ACTA Metrol Sinica, 2010, 31(5) 12]张蕊,祖丽亚,樊铁,等.测定胆固醇含量鉴别地沟油的研究门中国 油脂,2006,31(5)65-67 23]吴惠勤,黄晓兰,陈江韩,等. SPME/GC-MS鉴别地沟油新方法卩分 Zhang R, Zu LY, Fan T, et al. Distinguishing Illegal cooked oil in edible 析测试学报,2012,(31)1:1-6 regetable oil by determination of cholesterol content P]. China Oil Fat, Wu HQ, Huang XL, Chen JH, et al. A novel method for the identification 2006,31(565-67 of illegal cooked oil using SPME/GC-MS PJJ Instrum Anal, 2012, (31) 13]张亿,杨梅,陈红,等.微波萃取技术在食用植物油与潲水油中胆固醇 含量测定的应用中国卫生检验杂志,2011,21):1658-1660. 24]尹平河,王桂华,赵玲,等.GC-MS法鉴别食用油和餐饮业中废弃油脂 Zhang Y, Yang M, Chen H, et al. The application of microwave extraction 的研究分析试验室,2004,23(4)8-11. method on determination of cholesterol level in vegetable oils and waste Yin PH, Wang GL, Zhang L, et al. Study of recognition of edible oils and oils ]. Chin J Health Lab Technol, 2011, 21(7): 1658-1660. waste edible oils in the restaurants by GC-MS [J].Chin J Anal Lab, 2004, 「14]陈初良,张惠琴,甘云娟,等.食用植物油掺入动物油脂鉴别方法的研 粮油食品科技,2009,17(3):41-42 25]李晓英,彭德伟.餐饮废油与食用植物油品质的GCMS检测]中国 Chen CL, Zhang HQ, Gan YJ, et al. Study on the identification method of 油脂,2011,36(4):74-77 edible vegetable oil and animal oil incorporation P-Sci Technol Cereal Oil Li XY, Peng DWQuality analysis of cookingwaste oil and edible Food,2009,17341-42. vegetable oil by GC-MS P] China Oil Fat, 2011, 36(4): 74-77. 「15]刘庆菊,蔡波太,袁龙飞,等.基于高压液相色谱法的地沟油聚类分析26]黄军,熊华,李亮等.潲水油在精炼中卫生指标的检测与分析中 方法研究[食品安全质量检测学报,2013,4(2:401-4 国油脂,2008,3(10:70-74 Liu QJ, Cai BT, Yuan LF, et al. The clustering analysis of the illegal Huang J, Xiong H, Li L, et al. Hygiene indexes detection and analysis of cooked oil based on high pressure liquid chromatography []. J Food Saf hogwash oil in refining process P] China Oil Fat, 2008, 33(10): 70-74. Qual,2013,4(2):401-409 [27 Coeera M, Lopez O, Estelrich J, et al. Use of a fluorescence spectroscopy 6]王世成,范津杉,王颜红,等.液相色谱-大气压化学电离质谱分析鉴 technique to study the adsorption of sodium dodecy Sulfonate on 别地沟油中的氧化成分门分析化学,2014,(42)5:741-746 posomes ]. Chem Phys Lipid, 2001, 110: 19-26 Wang SC, Fan JS, Wang YH, et al. Determination of xidation products of 8]刘薇,尹平河,赵玲.荧光法测定十二烷基苯磺酸钠鉴别潲水油的研 lycerides in illegal cooked oil using high performance liquid 究门中国油脂,2005,30(524-26 chromatography-atmospheric pressure chemical ionization mass Liu W, Yin PH, Zhao L. Distinguishing hogwash fat by determination of spectrometry J]. Chin J Anal Chem, 2014, (42)5: 741-746 sodium dodecylbenzene sulfonate with fluorescence spectrum analysis P- 7赵海香,任荷玲,许秀丽等.应用脂肪酸甲酯快速筛选植物油中掺假 China Oil Fat, 2005, 30(5): 24-26 地沟油门食品科学,2014,(35)16:148-152. [29]张寒俊,汪海波,唐宇.同步荧光猝灭法测定地沟油中微量十二烷基 en HL x 苯磺酸钠[门分析仪器,2010,(6):43-46. adulteration in vegetable oil based on fatty acid methyl esters P]. Food Sci, Zhang H, Wang HB, Tang Y Determination of trace sodium dodecyl 16:148-152. enzence sulfonate in illegal cooked oil by synchronous fluorescence 「18]吉礼,车振明,李明元,电导率法快速甄别泔水油的研究门中国油脂, quenching spectrometry []. Anal Instrum, 2010,(6): 43-46.第 1 期 王 嵬, 等: 地沟油鉴别检测方法研究进展 223 军医大学学报, 2011, 33(13): 13661369. Ran L, Zhou Y, Zhu JD, et al. Acute toxicity and genetic toxicity of hogwash fat [J]. J Third Milit Med Univ, 2011, 33(13): 13661369. [8] 卢海燕, 王欣, 赵婷婷, 等. “地沟油”常见检测方法及低场核磁共振法 的研究进展[J]. 食品安全质量检测学报, 2013, 4(5): 14281436. Lu HY, Wang X, Zhao TT, et al. Research progress on the common detection methods and LF-NMR of illegal cooked oil [J]. J Food Saf Qual, 2013, 4(5): 14281436. [9] 胡小泓. 稍水油鉴别方法的研究[J]. 食品工业, 2010, 4: 98100. Hu XH. Study on the Identification method of Slightly water oil [J]. Food Ind, 2010, 4: 98100. [10] 王乐, 刘尧刚, 陈凤飞, 等. 地沟油的污染及变质情况研究[J]. 武汉工 业学院学报, 2007, 26(4): 14. Wang L, Liu YG, Chen FF, et al. Study on pollution and deterioration of the illegal cooked oil [J].J Wuhan Polytech Univ, 2007, 26(4):14. [11] 曹维金, 杨永存, 招辉, 等. 基于常规指标鉴别“地沟油”与食用植物油 的有效性评估卫生研究, 2014, (43)2: 311312. Chao WJ, Yang YC, Zhao H, et al. The effectiveness evaluation of based on the conventional indexes to identify " illegal cooked oil " and edible vegetable oil [J]. J Hyg Res, 2014, (43)2: 311312. [12] 张蕊, 祖丽亚, 樊铁, 等. 测定胆固醇含量鉴别地沟油的研究[J]. 中国 油脂, 2006,31(5): 6567. Zhang R, Zu LY, Fan T, et al. Distinguishing Illegal cooked oil in edible vegetable oil by determination of cholesterol content [J]. China Oil Fat, 2006, 31(5): 6567. [13] 张亿, 杨梅, 陈红, 等. 微波萃取技术在食用植物油与潲水油中胆固醇 含量测定的应用[J]. 中国卫生检验杂志, 2011, 21(7): 16581660. Zhang Y, Yang M, Chen H, et al. The application of microwave extraction method on determination of cholesterol level in vegetable oils and waste oils [J]. Chin J Health Lab Technol, 2011, 21(7): 16581660. [14] 陈初良, 张惠琴, 甘云娟, 等. 食用植物油掺入动物油脂鉴别方法的研 究[J]. 粮油食品科技, 2009, 17(3): 4142. Chen CL, Zhang HQ, Gan YJ, et al. Study on the identification method of edible vegetable oil and animal oil incorporation [J].Sci Technol Cereal Oil Food, 2009, 17(3): 4142. [15] 刘庆菊, 蔡波太, 袁龙飞, 等. 基于高压液相色谱法的地沟油聚类分析 方法研究[J]. 食品安全质量检测学报, 2013, 4(2): 401409. Liu QJ, Cai BT, Yuan LF, et al. The clustering analysis of the illegal cooked oil based on high pressure liquid chromatography [J]. J Food Saf Qual, 2013, 4(2): 401409. [16] 王世成, 范津杉, 王颜红, 等. 液相色谱-大气压化学电离质谱分析鉴 别地沟油中的氧化成分[J]. 分析化学, 2014, (42)5: 741746. Wang SC, Fan JS, Wang YH, et al. Determination of xidation products of lycerides in illegal cooked oil using high performance liquid chromatography-atmospheric pressure chemical ionization mass spectrometry [J]. Chin J Anal Chem, 2014, (42)5: 741746. [17] 赵海香, 任荷玲, 许秀丽, 等. 应用脂肪酸甲酯快速筛选植物油中掺假 地沟油[J]. 食品科学, 2014, (35)16: 148152. Zhao HX, Ren HL, Xu XL, et al. Rapid screening for gutter oil adulteration in vegetable oil based on fatty acid methyl esters [J]. Food Sci, 2014, (35)16: 148152. [18] 吉礼, 车振明, 李明元. 电导率法快速甄别泔水油的研究[J]. 中国油脂, 2009, 34(3): 7577. Ji L, Che ZM, Li MY. Rapid distinguishing of swill on by conductivity determination [J]. China Oil Fat, 2009, 34(3): 7577. [19] 彭进, 黄道平, 刘吉星, 等. 电导率的测定在鉴别潲水油中的应用研究 [J]. 实用预防医学, 2007, 14(3): 878879. Peng J, Huang DP, Liu JX, et al. Application study of electrical conductivity measurement in hogwash oil identification [J].Pr Pre Med, 2007, 14(3): 878879. [20] 胡小泓, 刘志金, 郑雪玉, 等. 应用电导率检测潲水油方法的研究[J]. 食品科学, 2007, 28(11): 482484. Hu XH, Liu ZJ, Zhen XY, et al. Research on elctroconductivity detection of hogwash fat [J]. Food Sci, 2007, 28(11): 482484. [21] 任佳丽, 刘振华, 李忠海, 等. 利用压电换能器快速鉴别潲水油[J]. 食 品与机械, 2011, 27(2): 6264. Ren JL, Liu ZH, Li ZW, et al. The rapid identification of swill oil by piezoelectric transducer [J]. Food Mach, 2011, 27(2): 6264. [22] 李红, 屠大伟, 李根容, 等. 固相微萃取及主成分分析用于潲水油 GC-MS 指纹图谱的分析[J]. 计量学报, 2010, 31(5): 101105. Li H, Tu DW, Li GR, et al. SPEM and principal component analysis of hogwash oil GC-MS fingerprint [J]. ACTA Metrol Sinica, 2010, 31(5): 101105. [23] 吴惠勤, 黄晓兰, 陈江韩, 等. SPME/GC-MS 鉴别地沟油新方法[J]. 分 析测试学报, 2012, (31)1: 16. Wu HQ, Huang XL, Chen JH, et al. A novel method for the identification of illegal cooked oil using SPME/GC-MS [J].J Instrum Anal,2012, (31)1: 16. [24] 尹平河, 王桂华, 赵玲, 等. GC-MS法鉴别食用油和餐饮业中废弃油脂 的研究[J]. 分析试验室, 2004, 23(4): 811. Yin PH, Wang GL, Zhang L, et al.Study of recognition of edible oils and waste edible oils in the restaurants by GC-MS [J].Chin J Anal Lab, 2004, 23(4): 811. [25] 李晓英, 彭德伟. 餐饮废油与食用植物油品质的 GC-MS 检测[J]. 中国 油脂, 2011, 36(4): 7477. Li XY, Peng DW.Quality analysis of cookingwaste oil and edible vegetable oil by GC-MS [J]. China Oil Fat, 2011, 36(4): 7477. [26] 黄军, 熊华, 李亮, 等. 潲水油在精炼中卫生指标的检测与分析[J]. 中 国油脂, 2008, 33(10): 7074. Huang J, Xiong H, Li L, et al.Hygiene indexes detection and analysis of hogwash oil in refining process [J]. China Oil Fat, 2008, 33(10): 7074. [27] Coeera M, .Lopez O, .Estelrieh J, et al. Use of a fluorescence spectroscopy technique to study the adsorption of sodium dodecy lsulfonate on liposomes [J].Chem Phys Lipid, 2001, 110: 1926. [28] 刘薇, 尹平河, 赵玲. 荧光法测定十二烷基苯磺酸钠鉴别潲水油的研 究[J]. 中国油脂, 2005, 30(5): 2426. Liu W, Yin PH, Zhao L. Distinguishing hogwash fat by determination of sodium dodecylbenzene sulfonate with fluorescence spectrum analysis [J]. China Oil Fat, 2005, 30(5): 2426. [29] 张寒俊, 汪海波, 唐宇. 同步荧光猝灭法测定地沟油中微量十二烷基 苯磺酸钠[J]. 分析仪器, 2010, (6): 4346. Zhang HJ, Wang HB, Tang Y. Determination of trace sodium dodecyl benzence sulfonate in illegal cooked oil by synchronous fluorescence quenching spectrometry [J]. Anal Instrum, 2010, (6): 4346