Heart as Strong as Iron\ Techniques Checklist: Use of a centrifuge Equipment: Disposable UV-Vis cuvettes 1-mL capacity) .Pipetmen: 20P, 100 P, 1000 P .Pipet tips Eppendorf tubes (safe-lock) .Hot plate
the Peach Get in the Banana?\ Techniques Checklist: Setting up distillation glassware correctly .Performing atmospheric pressure distillations Using Gas Chromatography(GC)to analyze samples Pre-lab Discussion and Required Reading:
Techniques Checklist m manifold use Manipulations under an inert atmosphere Solvent de-gassing Pre-Lab Discussion and required reading: Air sensitive techniques
1. Transfer and Extraction Techniques 1.1. Competent Chemist Rating:\Ethyl Ester's Excellent Adventure Techniques Checklist Extraction and Washing Careful transfer of solutions without loss of material Solvent drying and concentration Melting point determination
This handout describes standard extraction and washing protocols that can be applied to virtually any crude reaction mixture. Aqueous washings are done to remove water soluble impurities from organic products since normally the compound that you desire will be dissolved in Reference
