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Flash column chromatography is a quick and (usually) easy way to separate complex mixtures of compounds. We will be performing relatively large scale separations in 5.301,around 1.0 g of compound. Columns are often smaller in scale than this and some of you will experience these once you move into the research lab. Column chromatography uses the same principles
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WARNING NOTICE: The erperimants described in these matcrials are potantially hazardous and require a high level ofsafcty training special facilities and equipment, and supervision by appro responsibility, liability, and risk for the implemontation of such safey procedures and meastncs. MIT shall have no responsibility, liability, or risk for the content or implementation any of the matainl presented. Legal Notices
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将液体从固体中分开来的最简易方法是什么?过滤在此影片中 将学习如何有效的用重力过露及真空过滤来进行。 The easiest way to separate a liquid from a solid? Filtration! Learn how to effectively carry out gravity and vacuum filtrations in this video
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在本影片中学习如何熟悉滴定技术---用酚?在酸/碱滴定中的详 细示范。 Learn how to master the art of titration in this video-with a detailed demonstration of an acid/base titration using phenolphthalein
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薄层分析法在许多研究实业室是最常用的此影片将带领你每 步骤,从准备跑瓶到计算RF(retention factor)值 步骤, Thin-layer chromatography is the most commonly used analytical technique in many research labs. This video walks you through every step from setting up a developing chamber to calculating Rf values
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萃取、冲洗和干燥:还没到结束不能算结束。藉由分液漏斗示 。 范液相-液相萃取并学习如何用”反应检查步骤”检查你的反应。这 是一个你不会想错失的一个纯化技巧! Extracting, Washing and Drying: It ain't over 'til it's over. Learn how to \work up\ your reaction using a separatory funnel to perform a liquid-liquid extraction. This is one purification technique you don't want to miss!
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再结晶须有耐心,但它是值得的!此影片让你用一种溶剂与两种 溶剂的再结晶方法从溶解度测试到冷过滤来经验此过程 Recrystallization takes patience, but it's worth it! This video walks you through the procedure, from solubility tests to cold filtration, with information on one-solvent and two-solvent recrystallizations
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§3.1 概述 §3.2 寻址方式 §3.3 数据传送类指令(29条) §3.4 算术运算类指令(24条) §3.5 逻辑运算类指令(24条) §3.6 控制转移类指令( 17条) §3.7 位操作指令( 17条)
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一、分析零件图样 二、构成零件轮廓的几何条件 三、尺寸精度要求 四、形状和位置精度要求 五、表面粗糙度要求
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矩阵运算是数值计算中最重要的一类运算特别是在线性代数和数值分析中它是一种最 基本的运算。本章讨论的矩阵运算包括矩阵转置、矩阵向量相乘、矩阵乘法、矩阵分解以 及方阵求逆等。在讨论并行矩阵算法时分三步进行:①算法描述及其串行算法;②算法的 并行化及其实现算法框架以及简单的算法分析;③算法实现的MP源程序,以利于读者实 践操作
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