从固态到气态,然后直接回到固态。此纯化技巧既漂亮又实用 的。找出此影片中为什么用大气压力来升华二茂铁(Ferrocene) From solid to gas, and then straight back to solid. This purification technique is both beautiful and useful. Find out why by watching the atmospheric pressure sublimation of ferrocene in this video
使用旋转挥发仪:旋转挥发仪是你在实验室的好朋友。此影片 中将会确定你建立了一个安全并产生关系。 Using the Rotavap: The rotary evaporator is your friend in the lab. This video will ensure that you build a safe and productive relationship
不要让不精确在实验室阻碍你!此影片介绍正确方法来使用滴 管、滴定管、量瓶和注射器精确测量液体体积。 Don't let inaccuracy hold you back in lab! This video introduces the proper methods for measuring precise volumes of liquid using pipets, burets, volumetric flasks, and syringes
发现一些薄层分析法更复杂的技巧---剪玻璃TLC板,用火 焰造TLC染色剂点棍,使用TLC染色剂以使点显像。 Discover a few of the more complicatec skills related to thin layer chromatography cutting glass TLC plates, flame-pulling spotters, and using TLC stains to visualize spots
Overview: As you may discover, growing single crystals takes patience as well as an artful hand Crystallizations can be very sensitive to temperature and minor disturbances. Therefore, you will be encouraged to try several different temperatures using otherwise identical conditions, and to always find a quiet undisturbed location to promote crystal growth. Here are some tried and true tips to get