This handout describes how to prepare a standard gas chromatograph sample. It involves preparing a dilute solution of a somewhat volatile compound and using the GC to assess its purity
Heart as Strong as Iron\ Techniques Checklist: Use of a centrifuge Equipment: Disposable UV-Vis cuvettes 1-mL capacity) .Pipetmen: 20P, 100 P, 1000 P .Pipet tips Eppendorf tubes (safe-lock) .Hot plate
Techniques Checklist m manifold use Manipulations under an inert atmosphere Solvent de-gassing Pre-Lab Discussion and required reading: Air sensitive techniques
1. Transfer and Extraction Techniques 1.1. Competent Chemist Rating:\Ethyl Ester's Excellent Adventure Techniques Checklist Extraction and Washing Careful transfer of solutions without loss of material Solvent drying and concentration Melting point determination
