1. Transfer and Extraction Techniques 1.1. Competent Chemist Rating:\Ethyl Ester's Excellent Adventure Techniques Checklist Extraction and Washing Careful transfer of solutions without loss of material Solvent drying and concentration Melting point determination
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High temperature corrosion tests in 75%Na2SO4-25%. NaCl molten salt have been conducted on waspalloy specimens plasma sprayed with Co-Cr-B-Si, Ni-Cr-B-Si-hCr3C2, X-40, X-40 + TiC and Ni/Al + Al2O3 coatings, test coupons were exposed isothermally at 750℃up to 200 h. After the corrosion tests, each sample was examined by OM, SEM and EMPA. It was found that X-40, X-40 + TiC and Ni/Al + Al2O3 were violently corroded by the molten salt due to cracking and spalling of the coatings, whereas Co-Cr-B-Si and Ni-Cr-B-Si + Cr3C2 exhibited superior corrosion resistance, which were thought to be related to the formation of chromium and silicon oxide film. A possible corrosion mechanism had been proposed and it is suggested that the excellent corrosion resistance and high hot-hardness of the two B-Si containing coatings may be of significance for applications in petroleum refining industry as
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Working on a vacuum manifold: See LLP chapter 9.2 for an excellent discussion on working with air-sensitive reagents, including how to use a two-way manifold. De-gassing solvents: The best way to remove water and oxygen from a solvent is to distill it over an appropriate drying agent (such as sodium). This can sometimes be a lengthy (and dangerous)task. Since we
Question No. 1 A liquid Ni-Al alloy sphere is levitated with an induction coil in an excellent vacuum chamber at 500 C. Stirring of the droplet is intense so that the melt composition is uniform at any time. If the sphere has a radius of one cm and an initial Al mole fraction of 1%. Derive an expression which
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